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CERTIFICATE TIFICA TE OF ANALYSIS <br /> Qalytical Laboratory <br /> Friday,April 4, 2008 <br /> Attention: Guy W.Roy <br /> R&L Diesel <br /> P-0-8ox 2498 Report Page 31 of 41 <br /> Danville, CA 94526 <br /> Volatile Organic Ci6rnpounds bV EPA Method 8260B <br /> Sample Informatiln <br /> Sample I& B3 -29 Sample Type. Grab <br /> Laboratory ID- 8030609-07 <br /> Project Name.- UST-Waste Oil <br /> ,-J Date/Time Sampled. 06-Mar-08 14:15 by Guy W.Rpy Sample Matrix: Soil <br /> Test Parameter Result DLR Unit 0ifulion Batch Prepared Analysis Date Method votes <br /> Acetone NO 100 'ug/kg 1 AC81 102 11-Mar-08 11-Mar-08 EPA 8260E <br /> Benzene NO 2.00 i ug/kg 1 AC61102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Bromobenzene NO 2.00 1 AC61102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Bromochloromethane NO 2.00 ;ug/kg 1 AC61102 11-Mar-08 11-Mar-08 EPA 8260E <br /> Bromodichloromethane ND 2.00 ug/kg I AC61102 11-Mar-08 11-Mar-08 EPA 8260E <br /> Bromoform NO 2.00 ug/kg I AC61102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Bromomethane <br /> NO 2.00 iug/kg 1 AC61102 11-Mar-08 11-Mar-08 EPA 82606 <br /> 2-Butanone ND 20.0 ug/kg I AC41102 11-Mar-08 11-Mar-08 EPA 8260E <br /> n-Butylbenzene NO 2.00 ug/kg 1 AC8 1102 11-Mar-08 11-Mar-08 EPA 8260B <br /> sec-Butylbenzene NO 2.00 ug/kg 1 AC61102 11-Mar-08 I I-Mar-08 EPA 8250B <br /> tert-Butylbenzene ND 2.00 ugfkg 1 AC81 102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Carbon disulfide NO 20-0 ug/kg 1 AC81 102 11-Mar-08 I I-Mar-08 EPA 82608 <br /> . <br /> w, Carbon tetrachloride NO 2.00 ug/kg I AC61102 11-Mar-08 11-Mar-08 EPA 8260E <br /> rChiorobenzene NO 2.00 ug/kg I AC91 102 11-Ma r-08 11-Mar-08 EPA 8260E <br /> J-;, Chloroethane NO 2.00 ug/kg 1 AC61102 11-Mar-08 11-Mar-08 EPA 8260E <br />�J 2-Chloroethylvinyl ether NO 20-0 ug/kg 1 AC8 1102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Chloroform NO 2.00 ugtkg 1 AC61102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Chloromethane NO 2,00 u:glkg I AC81102 11-Mar-08 11-Mar-08 EPA 82608 <br /> 2-Chlorotoluene NO 2.00 ug/kg I AG81 102 11-Mar-08 11-Mar-08 EPA 8260B <br /> . <br /> 4-Chlorotoluene NO 2.00 ug/kg 1 AC61102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Dibromochloromethane ND 2.00 ug/kg I AC8 1102 11-Mar-08 11-Mar-08 EPA 8260B <br />�.q 1,2-Dibromo-3-chloropropene ND 2.00 ug/kg I AC61102 11-Ma r-08 11-Mar-08 EPA 8260B <br /> 1,2-Dibromoethane(EDB) NO 2.00 ug/kg 1 AC91 102 11-Mar-08 11-Mar-08 EPA 8260E <br /> 11 Dibromomethane NO 2.00 ug/kg I AC61102 11-Mar-08 11-Mar-08 EPA 8260E <br /> ' <br /> 1,2-Dichlorobenzene NO 2.00 ug/kg I— AC61102 11-Mar-08 I I-Mar-08 EPA 8260E <br /> 1,3-Dichlorobenzene NO 2.00 uglkg I ACE�11 102 11-Mar-08 11-Mar-08 EPA 82603 <br /> 1,4-Dichlorobenzene NO 2.00 ug/kg I AC8:1 102 11-Mar-08 I I-Ma r-08 EPA 8260B <br /> Dichlorodffluoramethane NO 2.00 ug/kg 1 Adl 102 11-Mar-08 11-Mar-08 EPA 8260B <br /> M-Dichloroethane NO 2.00 U;gfkg I AC81 102 11-Mar-08 11-Mar-08 EPA 8260B <br /> is mg1L=milligrams per Liter=ppm DLR=Defection LimisforPurpose of Reporting <br /> uglL=micrograms per Liter-pph Exceptional sample matrices or interferences may <br /> AKresult in higher defection limits. <br /> RESPECTFULLY SUBMITTED, <br /> 4 <br /> Jonathan Le,Laboratory Director <br /> 3935 N. Coronado Ave, Stockton,!CA 95204 Tel.: (209) 477-8105 Fax: (209) 546-7497 <br />