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conditions of drying shall be reported. <br /> (d) Samples shall be prepared for analysis for total content of substances listed in section 66261.24(a)(2)(B) as follows: <br /> (1) type is if the waste or other material is a millable solid, the sample shall be passed directly, or shall be milled to pass, through <br /> a one-millimeter standard sieve before it is analyzed. If the sample contains non-friable solid particles which do not pass directly <br /> through a one-millimeter sieve and which are extraneous and irrelevant as hazardous constituents to the waste or other <br /> material, they shall be removed to the extent feasible by mechanical means and discarded. Solids which remain in the waste or <br /> other material after removal of the aforesaid extraneous particles shall be milled to pass through a one-millimeter sieve and shall <br /> then be combined and mixed well with the solids which passed through the sieve without milling. The reconstituted sample shall <br /> then be analyzed as prescribed in this appendix; <br /> (2) type ii: if the waste or other material is a filterable mixture of liquid and solids in which the solids constitute five-tenths (0.5) <br /> percent by weight or greater of the sample, the liquid and solids shall be separated by filtration through a 0.45 micron membrane <br /> filter. The filtrate so obtained is to be designated as Initial Filtrate. Its volume is determined, and it is retained. The separated <br /> solids shall be sieved in a one-millimeter sieve and any nonfriable extraneous particles of the kinds described in subdivision (d) <br /> (1) of this appendix which do not pass through the sieve shall be removed to the extent feasible by mechanical means and <br /> discarded. The solids which remain after removal of the extraneous particles shall be milled to pass through a one-millimeter <br /> sieve and shall be recombined with solids which passed through the sieve without milling. This recombined solid material shall <br /> be extracted following the procedure in subdivision (g) of this appendix. A ratio of 10 milliliters of extraction solution per gram of <br /> solid shall be utilized with appropriate modifications for extraction vessel size. After completion of solids extraction, the filtered <br /> extractant is combined with Initial Filtrate, mixed thoroughly and analyzed as described in subdivision (9)(3) of this appendix; <br /> (3) type iii: if the waste or other material is a nonfilterable and nonmillable sludge, slurry, or oily, tarry or resinous material, it shall <br /> be analyzed as received unless it contains non-friable extraneous and irrelevant solid particles of the kinds described in <br /> subdivision (d)(1) of this appendix. If it contains such solid particles and they are of such size as not to pass through a one- <br /> millimeter sieve, they shall be removed to the extent feasible by mechanical means and discarded. The remainder of the sample <br /> shall be analyzed as prescribed in this appendix; <br /> (4) if it is necessary to dry a solid sample or the solids fraction of a sample before sieving, milling or removal of extraneous <br /> solids, or if a sample is dried prior to analysis, all weight losses due to drying shall be determined, and these losses and the <br /> conditions of drying shall be reported. <br /> (e) If the waste or other material is a liquid containing less than five-tenths (0.5) percent by weight of undissolved solids, it shall not <br /> be subject to the WET procedure, but shall be analyzed directly for the substances listed in section 66261.24(a)(2). The waste shall <br /> be classified as a hazardous waste if the total concentration in the waste of any substances listed in section 66261.24(a)(2) exceeds <br /> the TTLC value given for that substance. If, however, the total concentration is less than the TTLC but exceeds the STLC when <br /> expressed on a milligrams per liter basis, the waste or other material shall be filtered through a 0.45 micron membrane filter, the <br /> solids discarded and the filtrate shall be analyzed directly for the substances listed in section 66261.24(a)(2). The waste shall be <br />