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P=900 THA p TC] CERTIFICATE OFANALYSIS <br /> Analytical Laboratory <br /> 3935 N.Coronado Ave,Stockton CA.95204 Phone:(209)477-8105 <br /> Value Products Inc. Project Number: VP <br /> 2128 Industrial Drive Project Name: Powder Waste Water Tank Sample Work Order No.: <br /> Stockton,CA 95206 <br /> Project Manager: Doug Hall <br /> CAM-17 Metals by Method EPA6000/7000 Series-Quality Control <br /> Reporting Spike Somce <br /> Analyte Result Limit Units Level Result %REC RPD Notes <br /> Matrix Spike(A1193008-MS1) <br /> Antimony 0.10 0.010 mg/L 0.100 ND 105 <br /> Arsenic 0.30 0.010 " 0.100 0.17 133 QM4X <br /> SiNer 0.088 0.010 0.100 ND 88 <br /> Matrix Spike Dup(Atl93008-MSDI) <br /> Thallium 0.095 0.010.. mg/L 0.100 ND 95 2 <br /> Cadmium 0.095 0.0050 0.100 ND 95 3 <br /> Barium 0.14 0.050 0.100 0.043 97 3 <br /> Lead 0.096 0.010 0.100 ND 96 2 <br /> Mercury 0.052 0.0010. ND 5 <br /> Molybdenum 0.12 0.010 0.100 0.0083 115 3 <br /> Copper 0.35 0.050 0.100 0.073 275 2 QM-4X <br /> Zinc 1.7 OA50 " 0.100 15 191 1 QM-4X <br /> Anfnnony 0.11 0.010 0.100 ND 108 3 <br /> Vanadium 0.0988 0.0100 0.100 0.00884 90 3 <br /> Beryllitmr 0.090 0.010 " 0.100 ND 90 2 <br /> Cobalt 0.080 0.0050 0.100 ND 80 2 <br /> Selenium 0.10 0.010 0.100 ND 102 7 <br /> Chromium 0.11 0.010 0.100 0.021 88 3 <br /> Nickel 0.086 0.010 0.100 0.0094 77 2 <br /> Arsenic 0.31 0.010 0.100 0.17 142 3 QM-4X <br /> Silva 0.090 0.010 " 0.100 ND 90 2 <br /> Reference(AH93008-SRMI) <br /> Thallium 0.0080 0.010 mg/L 0.00845 94 <br /> Barium 1.3 0.050 1.02 126 <br /> Cadmium 0.038 0.0050 " 0.0389 98 <br /> Lead 0.033 0.010 0.0340 98 <br /> Vanadium 0.510 0.0100 0.408 125 <br /> Antimony 0.016 0.010 0.0164 99 <br /> Copper 0.22 0.050 0.225 97 <br /> Selenium 0.072 0.010 0.0703 102 <br /> Beryllium 0.0033 0.010 000321 101 <br /> Nickel 0.17 0.010 0.169 100 <br /> Mclybdenum 0.037 0.010 0.0377 99 <br /> Chromium 0.17 0.010 0.168 98 <br /> Approved By <br /> Precision Enviro-Tech. o California D.O.H.S.Cert.#2387 <br /> Page 6 of 8 <br />