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Oilfield Environmental and Compliance, INC. <br /> CalRecycle Project: PG5 <br /> 1001 I Street Project Number: 2512 Vineyard Ave Reported: <br /> Sacramento CA,95814 Project Manager: Glenn Young 10-May-13 14:39 <br /> Volatile Organic Compounds by EPA Method TO-15-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A305016-EPA TO-15 prep <br /> LCS Dup(A305016-BSDI) Prepared&Analyzed:01-May-13 <br /> Benzene 7.99 0.50 ppbv 10.0 79.9 63-130 3.44 25 <br /> Bromomethane 8.71 2.0 10.0 87.1 12-233 3.15 25 <br /> Carbon tetrachloride 8.40 0.50 10.0 84.0 61-130 3.64 25 <br /> Chlorobenzene 8.27 0.50 10.0 82.7 69-123 1.22 25 <br /> Chloroform 8.24 0.50 10.0 82.4 56-144 3.71 25 <br /> 1,2-Dibromoethane(EDB) 8.40 0.50 10.0 84.0 58-141 0.957 25 <br /> 1,3-Dichlorobenzene 7.98 0.50 10.0 79.8 34-182 0.377 25 <br /> 1,4-Dichlorobenzene 8.03 0.50 10.0 80.3 46-175 1.89 25 <br /> Dichlorodifluoromethane 8.31 0.50 10.0 83.1 53-168 0.604 25 <br /> 1,2-Dichloroethane 8.27 0.50 10.0 82.7 57-154 3.07 25 <br /> I,1-Dichloroethene 8.22 0.50 10.0 82.2 43-163 3.72 25 <br /> 1,2-Dichloropropane 8.35 0.50 10.0 83.5 61-130 3.91 25 <br /> Diisopropyl Ether 8.34 0.50 10.0 83.4 0-200 2.43 25 <br /> Ethanol 7.87 0.50 10.0 78.7 28-177 4.68 25 <br /> Ethylbenzene 8.06 0.50 10.0 80.6 53-139 1.12 25 <br /> Ethyl t-Butyl Ether 8.37 0.50 10.0 83.7 0-200 4.02 25 <br /> Methylene chloride 8.24 0.50 10.0 82.4 29-190 3.08 25 <br /> Methyl-t-butyl ether 8.41 0.50 10.0 84.1 58-145 4.13 25 <br /> Styrene 8.77 0.50 10.0 87.7 61-141 0.916 25 <br /> t-Amyl Methyl Ether 8.26 0.50 10.0 82.6 0-200 3.20 25 <br /> t-Butyl alcohol 7.97 0.50 10.0 79.7 0-200 4.10 25 <br /> Tetrachloroethene(PCE) 8.06 0.50 10.0 80.6 61-131 1.12 25 <br /> Toluene 6.88 0.50 10.0 68.8 60-131 1.76 25 <br /> 1,1,1-Trichloroethane 8.48 0.50 10.0 84.8 59-140 3.85 25 <br /> Trichloroethene(TCE) 8.09 0.50 10.0 80.9 66-131 2.50 25 <br /> Trichlorofluoromethane 8.36 0.50 10.0 83.6 52-155 3.04 25 <br /> Vinyl chloride 8.97 0.50 10.0 89.7 26-197 3.86 25 <br /> Xylenes(total) 23.3 0.50 30.0 77.6 60-139 2.30 25 <br /> Oilfield Environmental and Compliance The results in this report apply to the samples analysed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> TEL: (805) 922-4772 <br /> 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 <br /> Page 63 of 72 <br />