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Oilfield Environmental and Compliance, INC. <br /> CalRecycle Project: PG5 <br /> 10011 Street Project Number: 2512 Vineyard Ave Reported: <br /> Sacramento CA,95814 Project Manager: Glenn Young 10-May-13 14:39 <br /> Volatile Organic Compounds by EPA Method TO-15-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A305154-EPA TO-15 prep <br /> LCS Dup(A305154-BSDl) Prepared:07-May-13 Analyzed:08-May-13 <br /> Benzene 12.7 0.50 ppbv 10.0 127 63-130 15.8 25 <br /> Bromomethane 13.8 2.0 10.0 138 12-233 3.32 25 <br /> Carbon tetrachloride 13.2 0.50 10.0 132 61-130 16.1 25 QM-09 <br /> Chlorobenzene 13.3 0.50 10.0 133 69-123 15.6 25 QM-09 <br /> Chloroform 13.1 0.50 10.0 131 56-144 13.5 25 <br /> 1,2-Dibromoethane(EDB) 13.0 0.50 10.0 130 58-141 12.8 25 <br /> 1,3-Dichlorobenzene 12.4 0.50 10.0 124 34-182 15.0 25 <br /> 1,4-Dichlorobenzene 12.2 0.50 10.0 122 46-175 16.3 25 <br /> Dichlorodifluoromethane 14.3 0.50 10.0 143 53-168 0.845 25 <br /> 1,2-Dichloroethane 13.2 0.50 10.0 132 57-154 15.1 25 <br /> 1,1-Dichloroethene 12.8 0.50 10.0 128 43-163 9.38 25 <br /> 1,2-Dichloropropane 13.2 0.50 10.0 132 61-130 16.0 25 QM-09 <br /> Diisopropyl Ether 13.5 0.50 10.0 135 0-200 12.6 25 <br /> Ethanol 13.6 0.50 10.0 136 28-177 11.0 25 <br /> Ethylbenzene 12.7 0.50 10.0 127 53-139 14.2 25 <br /> Ethyl t-Butyl Ether 13.1 0.50 10.0 131 0-200 13.4 25 <br /> Methylene chloride 13.0 0.50 10.0 130 29-190 9.19 25 <br /> Methyl-t-butyl ether 13.1 0.50 10.0 131 58-145 11.6 25 <br /> Styrene 13.7 0.50 10.0 137 61-141 14.9 25 <br /> t-Amyl Methyl Ether 13.0 0.50 10.0 130 0-200 17.1 25 <br /> t-Butyl alcohol 12.8 0.50 10.0 128 0-200 9.17 25 <br /> Tetrachloroethene(PCE) 12.4 0.50 10.0 124 61-131 14.2 25 <br /> Toluene 10.7 0.50 10.0 107 60-131 13.3 25 <br /> 1,1,1-Trichloroethane 13.4 0.50 10.0 134 59-140 14.3 25 <br /> Trichloroethene(TCE) 12.9 0.50 10.0 129 66-131 13.0 25 <br /> Trichlorofluoromethane 13.1 0.50 10.0 131 52-155 7.59 25 <br /> Vinyl chloride 14.3 0.50 10.0 143 26-197 2.47 25 <br /> Xylenes(total) 36.3 0.50 30.0 121 60-139 14.5 25 <br /> Oilfield Environmental and Compliance The results in this report apply to the samples analyred in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> TEL: (805) 922-4772 <br /> 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 <br /> Page 70 of 72 <br />