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Page 3 of 3 Spargero Analytical Laboratory Division Mobile Laboratory Division TechnoboyInc. Scientific Division With Automation in Mind EPA Method 8260 GCMS Analysis Report Method Blank Attention: Mr. Steve Giacomini Date Sampled: Jul 7, 1999 EMCON Date Received: Jul 7, 1999 1433 North Market Blvd. Date Analyzed: Jul 10, 1999 Sacramento, CA 95834 Invoice# 11284JUL99 Project#: 16037-200.000 Project Name: Foothill Landfill, San Joaquin County Client ID: Method Blank LAB ID: QC-BATCH Matrix: Water Dilution 1: 1 Trace Name Concentration Concentration PQL MDL Units 56.) 1,3,5-trimethylbenzene ND ND 2.0 1.2 ug/L 57.) tert-butylbenzene ND ND 2.0 1.3 ug/L 58.) 1,2,4-trimethylbenzene ND ND 2.0 1.1 ug/L 59.) sec-butylbenzene ND ND 2.0 1.5 ug/L 60.) 1,3-dichlorobenzene ND ND 2.0 1.1 ug/L 61.) 1,4-dichlorobenzene ND ND 2.0 0.89 ug/L 62.) p-isopropyltoluene ND ND 2.0 1.2 ug/L 63.) 1,2-dichlorobenzene ND ND 2.0 0.95 ug/L 64.) n-butylbenzene ND ND 2.0 1.6 ug/L 65.) 1,2,-dibromo-3-chloropropane ND ND 2.0 1.2 ug/L 66.) 1,2,4-trichlorobenzene ND ND 2.0 1.1 ug/L 67.) Naphthalene ND ND 2.0 1.4 ug/L 68.) Hexachlorobutadiene ND ND 2.0 0.20 ug/L ' 69.) 1,2,3-trichlorobenzene ND ND 2.0 1.0 ug/L 70.) trans-1,4-dichloro-2-butene ND ND 2.0 1.3 ug/L ' Surrogate % Recovery of 1,2-dichloroethane-d4 = 101% Surrogate % Recovery of toluene-d8 99% Surrogate % Recovery of 4-Bromofluorobenzene = 97% ppb=parts per 6illion=ug1l=micrograms per liter ppm=parts per million=ug/ml=micrograms per milliliter ND=Not Detected. Compound(s)may be present at concentrations below the reporting limit. * =Trace Detected ' Jul 10, 1999 R. L.James,Principal Chemist Date Reported SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY (Certification No.1614) 8260MBW.xls 3050 Fite Circle, Suite 112 9 Sacramento, Colifomio 95827 0 (916) 362-8947 0 FAX(916) 362-0947