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Spargero <br /> Analytical Laboratory Division <br /> Mobile Laboratory Division <br /> Technologyinc. Scientific Division <br /> With Automation in Mind <br /> EPA Method 8260 GCMS <br /> Matrix Spike ( S) and Matrix Duplicate Spike (MSD) <br /> Attention: Mr. Steve Giacomini Date Sampled: Jul 7, 1999 <br /> EMCON Date Received: Jul 7, 1999 <br /> 1433 North Market Blvd. Date Analyzed: Jul 10, 1999 <br /> Sacramento, CA 95834 Invoice#: 11284JUL99 <br /> Project#: 16037-200.000 Project Name: Foothill Landfill, <br /> San Joaquin County <br /> Client ID: MS/MSD LAB ID: 11284-001MS/MSD <br /> Matrix: Water Dilution 1: 1 <br /> UNITS= ug/L <br /> Sample Spike MS MSD QC Limits <br /> Compound Conic Added MS MSD % Rec % Rec RPD RPD % Rec <br /> 1,1-Dichloroethene ND 50 39 37 78% 74% 5% 20 61-145 <br /> Benzene ND 50 42 40 84% 80% 5% 20 76-127 <br /> Trichloroethene ND 50 47 46 94% 92% 2% 20 71-135 <br /> ' Toluene ND 50 50 49 100% 98% 2% 20 76-130 <br /> Chlorobenzene ND 50 50 49 100% 98% 2% 20 75-130 <br /> ppb=parts per billion=ug/I=micrograms per liter <br /> ppm=parts per million=ug/ml=micrograms per milliliter <br /> ND=Not Detected. Compound(s)may be present at concentrations below the detection limit. <br /> r. <br /> Jul 10, 1999 <br /> R.L.James, Principal Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> ' 8260MSW.xis <br /> 3050 Fite Circle, Suite 112 • Sacramento, Colifomio 95827 9 (916) 362-8947 9 FAX(916) 362-0947 <br />