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Sequoia <br /> 819 Stoker Avenue,Suite 8 <br /> i.�y Sacramento.CA 95834 <br /> q ®14L (916)921-9640 <br /> FAX(916)921-0100 <br /> Analytical www-equoWabs.corn <br /> Shaw E&I-Sacramento Project Foothill Landfill,San Joaquin County S305696 <br /> 1326 N.Market Blvd. Project Number: 791289/00001000 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 06/06/03 16:09 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result ISL limit units Levet Result %REC Limits RPD Limit NOW <br /> Batch 3060097-EPA 5030B IP/TI <br /> Blank(3060097-BLKI) Prepared&Analyzed:06/05/03 <br /> Trichloroethene ND 0.36 0.50 ugn <br /> Trichlorofluorormdume ND 0.42 0.50 <br /> 1,2,3 Trichlotnpropane ND 0.55 1.0 " <br /> 1,2,4-Trimethylbenzene ND 0.18 0.50 <br /> 1,3,5 Trimethylbw=c ND 0.28 0.50 " <br /> Vinyl chloride ND 0.16 0.50 <br /> xylenes(total) ND 0.48 0.50 <br /> Surrogate:DibromoJluoromethane 12.1 25.0 . 89 70-130 <br /> Surrogate:1,2-DCA-d4 21.1 25.0 84 70-130 <br /> Surrogate:Toluene-d8 27.3 25.0 109 70-130 <br /> Surrogate.4-BFB 23.1 " 25.0 92 70-130 <br /> Laboratog Control Sample(3060097-BSl) Prepared&Analyzed:06/05/03 <br /> Benzene 19.0 0.28 0.50 ugA 25.0 76 70-130 <br /> Chlorobenzene 232 0.32 0.50 25.0 93 70-130 <br /> 1,1-Dichlotoethene - 18.9 0.24 0.50 *' 25.0 76 70-130 <br /> Toluene 25.0 0.32 0.50 25.0 100 70-130 <br /> Trichloroethene 19.8 0.36 0.50 25.0 79 70-130 <br /> Surrogate:DibromoJluoromethane 22.4 " 25.0 90 70-130 <br /> ' Surrogate:1,2 DCAd4 21.5 " 25.0 86 70-130 <br /> Surrogate.Toluene-& 16.3 2S.0 105 70-130 <br /> Surrogate.4-BFB 22.5 25.0 90 70-130 <br /> Matrix Spike(3060827-MSI) Source:S305696-01 Prepared:06/05/03 Analyzed:06/06/03 <br /> Benzene 19.1 028 0.50 ugil 25.0 ND 76 60-140 <br /> Chloroben=e 24.1 0.32 0.50 25.0 ND 96 60-140 <br /> l,l-Dichlomethene 19.5 ' 0.24 0.50 25.0 ND 78 60-140 <br /> Toluene 252 0.32 0.50 25.0 ND 101 60-140 <br /> Trichloroethene 20.2 0.36 0.50 25.0 ND 81 60-140 <br /> Surrogate:Dibromojluoromethane 22.1 25.0 89 70-130 <br /> Surrogate:1,2 DCAd4 11.3 25.0 85 70-130 <br /> Surrogate:Toluene-d8 26.6 25.0 106 70-130 <br /> Sur ogate:4:BFB .23.7 " 25.0 91 70-130 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody dodimert.This analytical report must be reproduced in its entirety. <br /> �\ Page 16 of 20 <br />