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COLUMBIA ANALYTICAL SERVICES, INC. <br />Client: Shaw Environmental & Infrastructure, Inc. Service Request No.: P0600115 <br />Project: Foothill Hollow Landfill/791289 (Leachate Module) Date Received: 2/2/07 <br />Sample Matrix: Water <br />CASE NARRATIVE <br />All analyses were performed consistent with the quality assurance program of Columbia Analytical Services, Inc. (CAS). This report <br />contains analytical results for samples designated for Tier II data deliverables. When appropriate to the method, method blank results <br />have been reported with each analytical test. Surrogate recoveries have been reported for all applicable organic analyses. Additional <br />quality control analyses reported herein include: Matrix/Duplicate Matrix Spike (MS/DMS), and Laboratory Control Sample (LCS). <br />Sample Receipt <br />The samples were received for analysis at Columbia Analytical Services on 2/2/07. Any discrepancies were noted upon initial <br />sample inspection, and recorded on the Client Notification Form included in this data package. The samples were received in <br />good condition and consistent with the accompanying chain of custody form. The samples were stored at 4°C upon receipt at the <br />laboratory. <br />Volatile Organic Compounds by EPA Method 8260B <br />Sample L-01 (P0700116-001) required dilution due to the presence of elevated levels of target analyte. The reporting limits are <br />adjusted to reflect the dilution. <br />Batch QC was run along with these samples. These results have been provided for informational purposes only. The upper control <br />criterion was exceeded for Trichlorofluoromethane in Laboratory Control Sample (LCS) PWG0700310-3. The analyte in question <br />was not detected in the associated field samples. The error associated with elevated recovery equates to a high bias. The sample data <br />is not significantly affected. No further corrective action was taken. <br />General Chemistry Parameters <br />The following sample was received and analyzed past the recommended holding time for Nitrate as Nitrogen: L-01 (P0700116- <br />001). The data has been flagged accordingly. <br />The Method Blank (MB) contained a trace hit of Chloride. The associated sample concentrations were greater than 20 times the <br />amount found in the MB; therefore, the data has not been significantly affected. No further corrective action was required. <br />Batch QC was run along with this sample. These results have been provided for informational purposes only. The Method <br />Blank and Laboratory Control Sample were within control criteria. <br />Approved by__ (lf �_ G /�� Date 'i 1/'9 <br />