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J <br />J <br />LI <br />Surroeate Name <br />Dibromofluoromethane <br />Toluene -d8 <br />4-Bromofluorobenzene <br />Comments: <br />Control Date <br />%Rec Limits Analyzed Note <br />109 77-126 02/13/07 Acceptable <br />104 77-119 02/13/07 Acceptable <br />94 74-121 02/13/07 Acceptable <br />Printed: 02/16/2007 08:34:31 Form I - Organic Page 3 of 3 <br />P:SnALTH\CRYSTAL.RPT\FormIm.pt Merged SuperSetReference: RR13372 <br />COLUMBIA ANALYTICAL SERVICES, INC. <br />Analytical Results <br />Client: <br />Shaw Environmental & Infrastructure, Inc <br />Service Request: P0700116 <br />Project: <br />Foothill Landfill, San Joaquin <br />County/791289 (Leachate Module) <br />Date Collected: NA <br />Sample Matrix: <br />Water <br />Date Received: NA <br />Volatile Organic Compounds <br />Sample Name: <br />Method Blank <br />Units: ug/L <br />Lab Code: <br />PWG0700310-4 <br />Basis: NA <br />Extraction Method: <br />EPA 5030B <br />Level: Low <br />Analysis Method: <br />8260B <br />Dilution <br />Date <br />Date <br />Extraction <br />Analyte Name <br />Result Q <br />PQL MDL Factor <br />Extracted <br />Analyzed <br />Lot Note <br />trans-1,3-Dichloropropene ND U <br />0.50 0.39 1 <br />02/13/07 <br />02/13/07 <br />PWG0700310 <br />trans-1,4-Dichloro-2-butene ND U <br />20 0.75 1 <br />02/13/07 <br />02/13/07 <br />PWG0700310 <br />Trichloroethene (TCE) <br />ND U <br />0.50 0.38 1 <br />02/13/07 <br />02/13/07 <br />PWG0700310 <br />Trichlorofluoromethane ND U <br />1.0 0.60 1 <br />02/13/07 <br />02/13/07 <br />PWG0700310 <br />Vinyl Acetate <br />ND U <br />10 0.90 1 <br />02/13/07 <br />02/13/07 <br />PWG0700310 <br />Vinyl Chloride <br />ND U <br />0.50 0.43 1 <br />02/13/07 <br />02/13/07 <br />PWG0700310 <br />J <br />J <br />LI <br />Surroeate Name <br />Dibromofluoromethane <br />Toluene -d8 <br />4-Bromofluorobenzene <br />Comments: <br />Control Date <br />%Rec Limits Analyzed Note <br />109 77-126 02/13/07 Acceptable <br />104 77-119 02/13/07 Acceptable <br />94 74-121 02/13/07 Acceptable <br />Printed: 02/16/2007 08:34:31 Form I - Organic Page 3 of 3 <br />P:SnALTH\CRYSTAL.RPT\FormIm.pt Merged SuperSetReference: RR13372 <br />