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COLUMBIA ANALYTICAL SERVICES, INC. <br />Analytical Results <br />Client: Shaw Environmental & Infrastructure, Inc <br />Project: Foothill Landfill, San Joaquin County/791289 (Ground Water) <br />Sample Matrix: Water <br />Sample Name: Method Blank <br />Lab Code: PWG0700304-4 <br />Extraction Method: EPA 5030B <br />Analysis Method: 8260B <br />Analyte Name <br />Vinyl Chloride <br />Volatile Organic Compounds <br />Dilution Date <br />Result Q PQL MDL Factor Extracted <br />ND U 0.50 .0.43 1 02/12/07 02/12/07 PWG0700304 <br />r <br />Service Request: <br />P0700115 <br />r <br />Date Collected: <br />NA <br />Control <br />Date <br />Date Received: <br />NA <br />Surrogate Name <br />%Rec <br />Limits <br />Analyzed <br />r <br />Units: <br />ug/L <br />Basis: <br />NA <br />Level: <br />Low <br />108 <br />77-126 <br />02/12/07 <br />Acceptable <br />Date Extraction <br />98 <br />Analyzed <br />Lot <br />Note_ <br />ND U 0.50 .0.43 1 02/12/07 02/12/07 PWG0700304 <br />r <br />Control <br />Date <br />Surrogate Name <br />%Rec <br />Limits <br />Analyzed <br />Note <br />Dibromofluoromethane <br />108 <br />77-126 <br />02/12/07 <br />Acceptable <br />Toluene -d8 <br />98 <br />77-119 <br />02/12/07 <br />Acceptable <br />4-Bromofluorobenzene <br />88 <br />74-121 <br />02/12/07 <br />Acceptable <br />1 <br />1 <br />r <br />r <br />r <br />r <br />r <br />1 <br />1 <br />Comments: <br />r <br />Printed: 02/16/2007 11:12:31 <br />Form I - Organic <br />Page 3 of 3 <br />P:\STEALTH\CRYSTAL.RPTTonnlm.rpt <br />Merged <br />SuperSetReference: RR13379 <br />