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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Results <br /> Client: Shaw Environmental&Infrastructure,Inc Service Request: P0700322 <br /> Project: Harney Lane Landfill,San Joaquin County/124593 (Ground Water) Date Collected: NA <br /> Sample Matrix: Water Date Received: NA <br /> Volatile Organic Compounds <br /> Sample Name: Method Blank Units: ug/L <br /> Lab Code: PWG0700543-4 Basis: NA <br /> Extraction Method: METHOD Level: Low <br /> Analysis Method: 624M <br /> Dilution Date Date Extraction <br /> Analyte Name Result Q PQL MDL Factor Extracted Analyzed Lot Note <br /> 1,1,1-Trichloroethane(TCA) ND U 0.50 0.46 1 04/05/07 04/05/07 PWG0700543 <br /> 1,1,2,2-Tetrachloroethane ND U 0.50 0.37 1 04/05/07 04/05/07 PWG0700541 <br /> 1,1,2-Trichloroethane ND U 0.50 0.40 1 04/05/07 04/05/07 PWG0700543 <br /> 1,1,2-Trichlorotrifluoroethanet. ND U 2:0 1.0 1 04/05/07 04/05/07 PWG0700543 <br /> 1,1-Dichloroethane ND U 0.50 0.35 1 04/05/07 04/05/07 PWG0700543 <br /> 1,1-Dichloroethene ND U 0.50 0.45 1 04/05/07 04/05/07 PWG0700543 <br /> 1,2-Dichlorobenzene ND U 0.50 0.36 1 04/05/07 04/05/07 PWG0700543 <br /> 1,2-Dichloroethane(EDC) ND U 0.50 0.33 1 04/05/07 04/05/07 PWG0700543 <br /> 1,2-Dichloropropane ND U 0.50 0.40 1 04/05/07 04/05/07 PWG0700543 <br /> 1,3-Dichlorobenzene ND U 0.50 0.33 1 04/05/07 04/05/07 PWG0700543 <br /> 1,4-Dichlorobenzene .ND U 0.50 0.37 1 04/05/07 04/05/07 PWG0700543 <br /> 2-Chloroethyl Vinyl Ether ND U 10 0.75 1 04/05/07 04/05/07 PWG0700543 <br /> Benzene ND U 0.50 0.42 1 04/05/07 04/05/07 PWG0700543 <br /> Bromodichloromethane ND U 1.0 0.40 1 04/05/07 04/05/07 PWG0700543 <br /> Bromoform ND U 1.0 0.41 1 04/05/07 04/05/07 PWG0700543 <br /> Bromomethane ND U 1.0 0.61 1 04/05/07 04/05/07 PWG0700543 <br /> Carbon Tetrachloride ND U 0.50 0.48 1 04/05/07 04/05/07 PWG0700543 <br /> Chlorobenzene ND U 0.50 0.36 1 04/05/07 04/05/07 PWG0700543 <br /> Chloroethane ND U 1.0 0.46 1 04/05/07 04/05/07 PWG0700543 <br /> Chloroform ND U 0.50 0:40 1 04/05/07 04/05/07 PWG0700543 <br /> Chloromethane ND U 1.0 0.40 1 04/05/07 04/05/07 PWG0700543 <br /> cis-1,2-Dichloroethenet ND U 0.50 0.39 1 04/05/07 04/05/07 PWG0700543 <br /> cis-1,3-Dichloropropene ND U 0.50 0.34 1 04/05/07 04/05/07 PWG0700543 <br /> Dibromochloromethane ND U 1.0 0.33 1 04/05/07 04/05/07 PWG0700543 <br /> Dichlorodifluoromethanet ND U 1.0 0.48 1 04/05/07 04/05/07 PWG0700543 <br /> Ethylbenzene ND U 0.50 0.41 1 04/05/07 04/05/07 PWG0700543 <br /> Total Xylenest ND U 1.5 1.1 1 04/05/07 04/05/07 PWG0700543 <br /> Methyl tert-Butyl Ethert ND U 2.0 0.71 1 04/05/07 04/05/07 PWG0700543 <br /> Methylene Chloride ND U 2.0 0.43 1 04/05/07 04/05/07 PWG0700543 . <br /> Tetrachloroethene(PCE) ND U 0.50 038 1 04/05/07 04/05/07 PWG0700543 <br /> Toluene ND U 0.50 0.36 1 04/05/07 04/05/07 PWG0700543 <br /> trans-1,2-Dichloroethene ND U 0.50 0.43 1 04/05/07 04/05/07 PWG0700143 <br /> trans-1,3-Dichloropropene ND U 0.50 0.39 1 04/05/07 04/05/07 PWG0700543 <br /> Trichloroethene(TCE) ND U 0.50 0.38 1 04/05/07 04/05/07 PWG0700543 <br /> method does not fall under the laboratory's NELAC certificate of approval. The method was modified(desorption time)to achieve the reporting limits. <br /> Comments: This rY PP <br /> 17 <br /> Printed: 04/09/2007 13:59:23 Form IA Organic Page 1 of 2 <br /> PASTE ALTMCRYSTAL.RPTTonnlm.tpt Merged SuperSetReference: RR13511 <br />