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Columbia Analytical Services,Inc. <br /> Sample Acceptance Check Form <br /> Client: Shaw Environmental&Infrastructure,Inc. Work order: P0802444 <br /> Project: Foothill Landfill,San Joaquin County/ 124591 (Ground Water) <br /> Sample(s)received on: 08/01/08 Date opened: 08/01/08 by: LKUKITA <br /> Note: This fort is used for all samples received by CAS. The use of this form for cu stody seals is strictly meant to indicate presence/absence and not as an indication of <br /> compliance or nonconformity. Thermal preservation and pH will only be evaluated either at the request of the client and/or as required by the method/SOP. <br /> Yes No NIA <br /> 1 Were sample containers properly marked with client sample ID? 0 ❑ ❑ <br /> 2 Container(s)supplied by CAS? 0 ❑ ❑ <br /> 3 Did sample containers arrive in good condition? 0 ❑ ❑ <br /> 4 Were chain-of-custody papers used and filled out? 0 ❑ ❑ <br /> 5 Did sample container Iabels and/or tags agree with custody papers? 0 ❑ ❑ <br /> 6 Was sample volume received adequate for analysis? 0 ❑ ❑ <br /> 7 Are samples within specified holding times? 0 ❑ ❑ <br /> 8 Was proper temperature(thermal preservation)of cooler at receipt adhered to? <br /> Cooler Temperature 3 °C Blank Temperature °C <br /> 9 Was a trip blank received? 0 ❑ ❑ <br /> Trip blank supplied by CAS: Serial# 070808 -TB 3 <br /> 10 Were custody seals on outside of cooler/Box? ❑ 0 ❑ <br /> Location of seal(s)? Sealing Lid? ❑ ❑ 0 <br /> Were signature and date included? ❑ ❑ 0 <br /> Were seals intact? ❑ ❑ <br /> Were custody seals on outside of sample container? ❑ 0 ❑ <br /> Location of seal(s)? Sealing Lid? ❑ ❑ 0 <br /> Were signature and date included? ❑ ❑ 0 <br /> Were seals intact? ❑ ❑ 0 <br /> 11 Do containers have appropriate preservation, according to method/SOP or Client specified information? 0 ❑ ❑ <br /> Is there a client indication that the submitted samples are pH preserved? 0 ❑ ❑ <br /> Were VOA vials checked for presence/absence of air bubbles? 0 ❑ ❑ <br /> Does the client/method/SOP require that the analyst check the sample pH and if necessary alter it? 0 ❑ ❑ <br /> 12 Tubes: Are the tubes capped and intact? ❑ ❑ 0 <br /> Do they contain moisture? ❑ ❑ 0 <br /> 13 Badges: Are the badges properly capped and intact? ❑ ❑ 0 <br /> Are dual bed badges separated and individually capped and intact? ❑ ❑ 0 <br /> ..........:::.....:.::::.::.::..:..:.:.. <br /> ------------------------ <br /> .... .... .. .:......... ..........................::::•,:..:....:�t.�.{.............�:::.�::::nom:::::;:....n.......�..�.•..�....�..�..(..............:1..:..n.:::::...,....rSil:::w4.:.i:•:5:::.wS�:�::p::�::1:::�vr:.::w:::::n•4�r. <br /> .;':.:;;•:;.:'.:::;:.;::::;:::.:::..:�:.:::.;'<.;;:.::.;:.::.�::;;:.;:�� "��!#3>:::::-::i'•.�i is .,..::::::::: <br /> .CRM1ti{GF.(l�'r�i.'i?i>Y•i:+:4i Si:+�i::iii:vi <br /> P0802444-001.01 40ml VOA HCL <2 A <br /> P0802444-001.02 40ml VOAHCL <2 A <br /> P0802444-001.03 40m1 VOA HCL A <br /> P0802444-001.04 100omL Plastic NP <br /> P0802444-001.05 250mL Plastic NP <br /> P0802444-001.06 500ml-Plastic HNO3 <2 <br /> .P0802444-002.01 40m1 VOA HCL <2 A <br /> Bxplain any discrepancies:(include lab sample ID numbers): <br /> *Required pH:Phenols/COD/NH3tTOC/rOX/NO3+NO2/rKN/r.PHOS,H2SO4(pH<2);Metals,HNO3(pH<2);CN(NaOH or NaOH/Asc Acid)(pH>12); <br /> Diss.Sulfide,NaOH(pH>12);T.Sulfide,NaOH/LnAc(pH>12) RSK-MEEPP,HCL(p11<2);RSK-CO2,(pH 5-8);Sulfur(pH>4) <br /> P0802444 Shaw Environmental&inf-astnicture,Ine._Poodull LandfUL San Joaquin County-124591(Ground Water)-Page t of 2 08/13/08 4:55 PM <br />