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r <br />L <br />C <br />C <br />�j <br />L <br />�1 <br />L <br />u <br />Ci <br />II <br />rI <br />L <br />1� <br />GA1*r <br />Toxics LTD. <br />AN ENVIRONMENTAL ANALYTICAL LABORATORY <br />Client Sample ID; SG 10 <br />Lab ID#: 0901481-IOA <br />MODIFIED EPA METHOD TO -14A GC/MS FULL SCAN <br />File Name: r012918 Date of Collection: 1/23/09 <br />Dil. Factor: 14.5 Date of Analysis: 1/29/09 08:13 PM <br />Container Type:1 Liter Summa Canister <br />Method <br />Surrogates %Recovery Limits <br />1,2-Dichloroethane-d4 88 70-130 <br />Toluene -d8 99 70-130 <br />4-Bromofluorobenzene 112 70-130 <br />Page 33 of 51 <br />Rpt. Limit <br />Amount <br />Rpt. Limit <br />Amount <br />Compound <br />(ppbv) <br />(ppbv) <br />(uG/m3) <br />(uG/m3) <br />1,1,2 -Trichloroethane <br />7.2 <br />Not Detected <br />40 <br />Not Detected <br />Tetrachloroethene <br />7.2 <br />42 <br />49 <br />280 <br />2-Hexanone <br />29 <br />Not Detected <br />120 <br />Not Detected <br />Dibromochloromethane <br />7.2 <br />Not Detected <br />62 <br />Not Detected <br />1,2-Dibromoethane (EDB.) ....................................................... <br />�:2..................................Not.Detected................................. <br />56..................................No...Detected.......... <br />Chlorobenzene <br />7.2 <br />Not Detected <br />33 <br />Not Detected <br />Ethyl Benzene <br />7.2 <br />Not Detected <br />31 <br />Not Detected <br />m,p-Xylene <br />7.2 <br />Not Detected <br />31 <br />Not Detected <br />o -Xylene <br />7.2 <br />Not Detected <br />31 <br />Not Detected <br />Styrene ..................................................................................................................................................................................................................................... <br />7.2 <br />Not Detected <br />31 <br />Not Detected <br />Bromoform <br />7.2 <br />Not Detected <br />75 <br />Not Detected <br />Cumene <br />7.2 <br />Not Detected <br />36 <br />Not Detected <br />1,1,2,2 -Tetrachloroethane <br />7.2 <br />Not Detected <br />50 <br />Not Detected <br />Propylbenzene <br />7.2 <br />Not Detected <br />36 <br />Not Detected <br />4-Ethyltoluene <br />......................................•--....-----....................................................................................................................................................................................................................................................................... <br />7.2 <br />Not Detected <br />36 <br />Not Detected <br />1,3,5-Trimethylbenzene <br />7.2 <br />Not Detected <br />36 <br />Not Detected <br />1,2,4-Trimethylbenzene <br />7.2 <br />Not Detected <br />36 <br />Not Detected <br />1,3 -Dichlorobenzene <br />7.2 <br />Not Detected <br />44 <br />Not Detected <br />1,4 -Dichlorobenzene <br />7.2 <br />Not Detected <br />44 <br />Not Detected <br />alpha-Chlorotoluene.....................................................................7:�.................................Not <br />Detected.................................38..................................Not <br />.............. <br />Detected.......... <br />1,2 -Dichlorobenzene <br />7.2 <br />Not Detected <br />44 <br />Not Detected <br />1,2,4-Trichlorobenzene <br />29 <br />Not Detected <br />220 <br />Not Detected <br />Hexachlorobutadiene <br />29 <br />Not Detected <br />310 <br />Not Detected <br />Container Type:1 Liter Summa Canister <br />Method <br />Surrogates %Recovery Limits <br />1,2-Dichloroethane-d4 88 70-130 <br />Toluene -d8 99 70-130 <br />4-Bromofluorobenzene 112 70-130 <br />Page 33 of 51 <br />