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COLUMBIA ANALYTICAL SERVICES, INC. <br />Analytical Results <br />Client: Shaw Environmental & Infrastructure, Inc Service Request: P0700704 <br />Project: Foothill Landfill, San Joaquin County (New Wells)/124591 Date Collected: 07/31/2007 <br />Sample Matrix: Water Date Received: 08/01/2007 <br />n <br />0 <br />Comments: <br />Printed: 08/15/2007 07:41:11 Form i A - Organic Page 3 of 3 <br />PaSTI:ALTH\CRYSTAL.IZP'AFomilm.ipt Merged SuperSetReference; RRI3820 <br />Volatile Organic CompoundsSample <br />Name: TRIP BLANK <br />Units: ug/L <br />Lab Code: P0700704-003 <br />Basis: NA <br />Extraction Method: EPA 503013 <br />Level: Low <br />Analysis Method: 8260B <br />Analyte Name <br />Result Q <br />PQL MDL <br />Dilution <br />Factor <br />Date <br />Extracted <br />Date <br />Analyzed <br />Extraction <br />Lot Note <br />Propionitrile <br />ND U <br />50 11 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />sec-Butylbenzene <br />ND U <br />1.0 0.37 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG070I151 <br />Styrene <br />ND U <br />0.50 0.37 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701I51 <br />tert-Amyl Methyl Ether <br />ND U <br />2.0 0.72 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />tert-Butyl Alcohol <br />ND U <br />20 8.7 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />tert-Butyl Ethyl Ether <br />ND U <br />2.0 0.64 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />tert-Butylbenzene <br />ND U <br />1.0 0.41 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Tetrachloroethene (PCE) <br />ND U <br />0.50 0.38 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Toluene <br />ND U <br />0.50 0.36 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />trans-l,2-Dichloroethene <br />ND U <br />0.50 0.43 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />trans-l,3-Dichloropropene <br />ND U <br />0.50 0.39 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />trans- l,4-DichIoro-2-butene <br />ND U <br />20 0.75 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Trichloroethene (TCE) <br />ND U <br />0.50 0.38 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Trichlorofluoromethane <br />ND U <br />1.0 0.60 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Vinyl Acetate <br />ND U <br />10 0.90 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Vinyl Chloride <br />ND U <br />0.50 0.43 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />_ <br />Control <br />Date <br />Surrogate Name <br />%Rec <br />Limits <br />Analyzed <br />Note <br />Dibromofluoromethane <br />96 <br />73-129 <br />08/08/07 <br />Acceptable <br />Toluene -d8 <br />101 <br />76-122 <br />08/08/07 <br />Acceptable <br />4-Bromofluorobenzene <br />95 <br />63-118 <br />08/08/07 <br />Acceptable <br />n <br />0 <br />Comments: <br />Printed: 08/15/2007 07:41:11 Form i A - Organic Page 3 of 3 <br />PaSTI:ALTH\CRYSTAL.IZP'AFomilm.ipt Merged SuperSetReference; RRI3820 <br />