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COLUMBIA ANALYTICAL SERVICES, INC. <br />Comments: <br />A J <br />Printed: 08/15/2007 07:41:13 Form I A - Organic Page 2 of 3 <br />P:15rEALTRNCRYS.-AL.RPT'%Fonnlm.ipt 1,1erged SuperSe(Reference: RR13820 <br />Analytical Results <br />Client: Shaw Environmental & Infrastructure, Inc <br />Service Request: P0700704 <br />Project: Foothill Landfill, San Joaquin County (New <br />We11s)/124591 <br />Date Collected: <br />NA <br />Sample Matrix: Water <br />Date Received: NA <br />r <br />Volatile Organic Compounds <br />Sample Name: Method Blank <br />Units: ug/L <br />Lab Code: PWG0701151-4 <br />Basis: NA <br />Extraction Method: EPA 5030B <br />Analysis Method: 8260E <br />Level: Low <br />Dilution <br />Date <br />Date <br />Extraction <br />Analyte Name <br />Result Q <br />PQL <br />MDL <br />Factor <br />Extracted <br />Analyzed <br />Lot Note <br />Bromobenzen.e <br />ND U <br />1.0 <br />0.40 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Bromochloromethane <br />ND U <br />0.50 <br />0.40 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Bromodichloromethane <br />ND U <br />1.0 <br />0.40 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Bromoform <br />ND U <br />1.0 <br />0.41 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Bromomethane <br />ND U <br />1.0 <br />0.61 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Carbon Disulfide <br />ND U <br />2.0 <br />0.83 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Carbon Tetrachloride <br />ND U <br />0.50 <br />0.48 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Chlorobenzene <br />ND U <br />0.50 <br />0.36 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Chloroethane <br />ND U <br />1.0 <br />0.46 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Chloroform <br />ND U <br />0.50 <br />0.40 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Chloromethane <br />ND U <br />1.0 <br />0.40 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Chloroprene <br />ND U <br />5.0 <br />1.0 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />cis-1,2-Dichloroethene <br />ND U <br />0.50 <br />0.39 <br />1 <br />08/08/07- <br />08/08/07 <br />PWG0701151 <br />cis-1,3-Dichloropropene <br />ND U <br />0.50 <br />0.34 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701.151 <br />cis-1,4-Dichloro-2-butene <br />ND U <br />20 <br />1.1 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Dibromochloromethane <br />ND U <br />1.0 <br />0.33 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701.151 <br />Dibromomethane <br />ND U <br />0.50 <br />0.39 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG070115I <br />_ <br />Dichlorodifluoromethane <br />ND U <br />1.0 <br />0.48 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Diisopropyl Ether <br />ND U <br />2.0 <br />0.66 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Ethanol <br />ND U <br />100 <br />73 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701I51 <br />Ethyl Methacrylate <br />ND U <br />5.0 <br />0.85 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Ethylbenzene <br />ND U <br />0.50 <br />0.41 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Hexachlorobutadiene <br />ND U <br />1.0 <br />0.46 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />lodomethane <br />ND U <br />10 <br />0.77 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Isobutyl Alcohol <br />ND U <br />100 <br />24 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Isopropylbenzene <br />ND U <br />1.0 <br />0.34 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Total Xylenes <br />ND U <br />1.5 <br />1.1 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Methacrylonitrile <br />ND U <br />50 <br />9.1 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701.151 <br />Methyl Methacrylate <br />ND U <br />5.0 <br />0.75 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Methyl tert-Butyl Ether <br />ND U <br />2.0 <br />0.71 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Methylene Chloride <br />ND U <br />2.0 <br />0.43 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />n-Butyibenzene <br />ND U <br />1.0 <br />0.37 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />n-Propylbenzene <br />ND U <br />1.0 <br />0.41 <br />1 <br />08/08/07 <br />08/08/07 <br />PWO0701151 <br />Naphthalene <br />ND U <br />1.0 <br />0.36 <br />1 <br />08/08/07 <br />08/08/07 <br />PWG0701151 <br />Comments: <br />A J <br />Printed: 08/15/2007 07:41:13 Form I A - Organic Page 2 of 3 <br />P:15rEALTRNCRYS.-AL.RPT'%Fonnlm.ipt 1,1erged SuperSe(Reference: RR13820 <br />