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Lab ID#: 1003147-11A <br />MODIFIED EPA METHOD TO -14A GUMS FULL SCAN <br />File Name: 6030911 Date of Collection: 2/2/10 3:57:00 PM <br />Dil. Factor: 2.33 Date of Analysis: 3/10/10 09:34 AM <br />J = Estimated value due to bias in the CCV. <br />Container Type: 1 Liter Summa Canister <br />Method <br />Surrogates %Recovery Limits <br />1,2-Dichloroethane-d4 111 70-130 <br />Toluene -d8 106 70-130 <br />4-Bromofluorobenzene 91 70-130 <br />Page 33 of 55 <br />Rpt. Limit <br />Amount <br />Rpt. Limit <br />Amount <br />Compound <br />(ppbv) <br />(ppbv) <br />(ug/m3) <br />(ug/m3) <br />1,1,2 -Trichloroethane <br />1.2 <br />Not Detected <br />6.4 <br />Not Detected <br />Tetrachloroethene <br />1.2 <br />2.3 <br />7.9 <br />15 <br />2-Hexanone <br />4.7 <br />Not Detected <br />19 <br />Not Detected <br />Dibromochloromethane <br />1.2 <br />Not Detected <br />9.9 <br />Not Detected <br />1,2-Dibromoethane (EDB) <br />1.2 <br />Not Detected <br />9.0 <br />Not Detected <br />Chlorobenzene <br />1.2 <br />Not Detected <br />5.4 <br />Not Detected <br />Ethyl Benzene <br />1.2 <br />Not Detected <br />5.0 <br />Not Detected <br />m,p-Xylene <br />1.2 <br />Not Detected <br />5.0 <br />Not Detected <br />o -Xylene <br />1.2 <br />Not Detected <br />5.0 <br />Not Detected <br />Styrene <br />1.2 <br />Not Detected <br />5.0 <br />Not Detected <br />Bromoform <br />1.2 <br />Not Detected <br />12 <br />Not Detected <br />Cumene <br />1.2 <br />Not Detected <br />5.7 <br />Not Detected <br />1,1,2,2 -Tetrachloroethane <br />1.2 <br />Not Detected <br />8.0 <br />Not Detected <br />Propylbenzene <br />1.2 <br />Not Detected <br />5.7 <br />Not Detected <br />4-Ethyltoluene <br />1.2 <br />Not Detected <br />5.7 <br />Not Detected <br />1,3,5-Trimethylbenzene <br />1.2 <br />Not Detected <br />5.7 <br />Not Detected <br />1,2,4-Trimethyl benzene <br />1.2 <br />Not Detected <br />5.7 <br />Not Detected <br />1,3 -Dichlorobenzene <br />1.2 <br />Not Detected <br />7.0 <br />Not Detected <br />1,4 -Dichlorobenzene <br />1.2 <br />Not Detected <br />7.0 <br />Not Detected <br />alpha-Chlorotoluene <br />1.2 <br />Not Detected <br />6.0 <br />Not Detected <br />1,2 -Dichlorobenzene <br />1.2 <br />Not Detected <br />7.0 <br />Not Detected <br />1,2,4-Trichlorobenzene <br />4.7 <br />Not Detected <br />34 <br />Not Detected <br />Hexachlorobutadiene <br />4.7 <br />Not Detected <br />50 <br />Not Detected <br />J = Estimated value due to bias in the CCV. <br />Container Type: 1 Liter Summa Canister <br />Method <br />Surrogates %Recovery Limits <br />1,2-Dichloroethane-d4 111 70-130 <br />Toluene -d8 106 70-130 <br />4-Bromofluorobenzene 91 70-130 <br />Page 33 of 55 <br />