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March 23, 2011 Lab ID : STK 1131554 <br />San Joaquin County Solid Waste Customer :3-2956 <br />Quality Control - Inorganic <br />constituent <br />Method <br />Date" <br />Type <br />Units <br />Cone. <br />QC Data <br />DQO <br />Note <br />Wet Chem <br />E. C. <br />2510B <br />02/22/2011:202034 <br />Blank <br />umhos/cm <br />ND <br /><1 <br />(SP 1101775-001) <br />Dup <br />umhos/cm <br />0.0% <br />0372 <br />Solids, Total Dissolved <br />2540 G <br />02/23/2011:202079 <br />Blank <br />mg/L <br />6.3 <br />20 <br />LCS <br />mg/L <br />995.0 <br />94.1% <br />90-110 <br />(STK1131572-W1) <br />Du <br />0.2% <br />10.0 <br />Chloride <br />300.0 <br />02125/2011:202195 <br />LCS <br />mg/L <br />25.00 <br />102% <br />90-110 <br />MS <br />mg/L <br />500.0 <br />105% <br />86-128 <br />(SP 1101904-001) <br />MSD <br />mg/L <br />500.0 <br />103% <br />86-128 <br />MSRPD <br />m <br />100.0 <br />1.1% <br />23.0 <br />300.0 <br />02/25/2011:203022 <br />CCB <br />ppm <br />0S9 <br />1 <br />CCV <br />ppm <br />25.00 <br />107% <br />90-110 <br />CCB <br />ppm <br />0.49 <br />1 <br />CCV <br />PPM <br />25.00 <br />106% <br />90-110 <br />ulfate <br />300.0 <br />02/25/2011:202195 <br />LCS <br />mg/L <br />50.00 <br />103% <br />90-110 <br />MS <br />mg/L <br />1000 <br />107% <br />78-137 <br />(SP 1101904-001) <br />MSD <br />mg/L <br />1000 <br />104% <br />78-137 <br />MSRPD <br />m <br />100.0 <br />2.5% <br /><12.3 <br />300.0 <br />02/25/2011:203022 <br />CCB <br />ppm <br />0.17 <br />2 <br />CCV <br />ppm <br />50.00 <br />106% <br />90-110 <br />CCB <br />ppm <br />-0.007 <br />2 <br />Litrate <br />CCV <br />PPM <br />50.00 <br />105% <br />90-110 <br />+ Nitrite as N <br />4500NO3F <br />MS <br />mg/L <br />4.000 <br />96.8% <br />5-285 <br />(STK1131454-001) <br />MSD <br />mg/L <br />4.000 <br />100% <br />5-285 <br />MSRPD <br />m <br />4.000 <br />3.0% <br />:530.4 <br />450ONO3F <br />02/21/2011:202617 <br />CCB <br />mg/L <br />-0.039 <br />0.1 <br />CCV <br />mg/L <br />4.000 <br />90.8% <br />90-110 <br />CCB <br />mg/L <br />-0.045 <br />0.1 <br />CCV I <br />mgtL 1 <br />4.000 1 <br />91.9% 1 <br />90-110 <br />Definition <br />ICV : Initial Calibration Verification - Analyzed to verify the instrument calibration is within criteria. <br />1CB : Initial Calibration Blank - Analyzed to verify the instrument baseline is within criteria. <br />CCV : Continuing Calibration Verification - Analyzed to verify the instrument calibration is within criteria. <br />CCB : Contmuing Calibration Blank - Analyzed to verify the instrument baseline is within criteria. <br />Blank : Method Blank - Prepared to verify that Bre preparation process is not contributing contamination to the samples. <br />I.CS :1,aboratory Control Standard/Sample - Prepared to verify that the preparation process is not affecting analyte recovery. <br />MS : Matrix Spikes -A random sample is spiked with a known amount of analyte. The reveries are an indication of how that sample <br />matrix affects analyte recovery. <br />MSD : Matrix Spike Duplicate of MS/MSD pair - A random sample duplicate is spiked with a known amount of analyted. The recoveries <br />are an indication of how that sample matrix affects analyte recovery. <br />Dup : Duplicate Sample - A random sample with each batch is prepared and analyzed in duplicate. The relative percent difference is an <br />indication of precision for the preparation and analysis. <br />: MS/MSD Relative Percent Difference (RPD) - The MS relative percent difference is an indication of prenision for the preparation <br />jMSR,D <br />and analysis. <br />ND : Non -detect - Result was below the DQO listed for the analyte. <br />DQO : Data Quality Objective - Ibis is the criteria a "nst which the qucontrol data is cora <br />Page 14 of 18 <br />