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® January 3,2013 <br /> San Joaquin County PWD-Solid Waste Div. Lab ID : STK1251217 <br /> Attn: Michael Carroll Customer 3-2956 <br /> 1810 E. Hazelton St. <br /> Stockton,CA 95205 <br /> Laboratory Report <br /> Introduction: This report package contains total of 23 pages divided into 3 sections: <br /> Case Narrative (2 pages) : An overview of the work performed at FGL. <br /> Sample Results (10 pages) : Results for each sample submitted. <br /> Quality Control (11 pages) : Supporting Quality Control (QC)results. <br /> Case Narrative <br /> This Case Narrative pertains to the following samples: <br /> Sample Description Date Date FGL Lab ED# Matrix <br /> Sampled Received <br /> FH-SW-UP- 12/05/2012 12/05/2012 STK1251217-001 Sw <br /> FH-SW-DWN- 12/05/2012 12/05/2012 STK1251217-002 Sw <br /> Sampling and Receipt Information: All samples were received,prepared and analyzed within the <br /> method specified holding times.All samples arrived on ice.All samples were checked for pH if acid or <br /> base preservation is required(except for VOAs).For details of sample receipt information,please see <br /> the attached Chain of Custody and Condition Upon Receipt Form. <br /> Quality Control: All samples were prepared and analyzed according to the following tables: <br /> Inorganic-Metals QC <br /> 200.7 12/12/2012:218281 All analysis quality controls are within established criteria. <br /> 12/11/2012:213717 All preparation quality controls are within established criteria,except: <br /> 3010 The following note applies to Sodium: <br /> 430 Post Digestion Spike(PDS)not within Acceptance Range(AR)because of matrix interferences <br /> affecting this analyte. <br /> Organic QC <br /> 12/06/2012:213587 All preparation quality controls are within established criteria,except: <br /> The following note applies to Acrolein,tert-Butanol: <br /> 5030B 310 LCS above Acceptance Range(AR).Samples which were non detect for this analyte were accepted. <br /> The following note applies to Acetone,Acrolein,Acrylonitrile,2-Butanone(MEK): <br /> ,435 Sample matrix may be affecting this analyte.Data was accepted based on the LCS or CCV recovery. <br /> weac., Page 1 of 23 <br /> Corporate Offices&Laboratory Office&Laboratory Office&Laboratory Office&Laboratory Field Office <br /> 853 Corporation Street 2500 Stagecoach Road 563 E.Undo Avenue 3442 Empresa Drive,Suite D Visalia,California <br /> Santa Paula,CA 93060 Stockton,CA 95215 Chico,CA 95926 San Luis Obispo,CA 93401 TEL:(559)734-9473 <br /> TEL:(805)392-2000 TEL(209)942-0182 TEL:(530)343-5818 TEL:(805)783-2940 Mobile:(559)737-2399 <br /> Env FAX:(8D5)525-4172/Ag FAX:(805)392-2063 FAX(209).942-0423 FAX:(530)343-3807 FAK(805)525-4172 FAX:(559)734-8435 <br /> CA NELAP Certification No.01110CA CA ELAP Certification No.1563 CA ELAP Certification No.2670 CA FLAP Certification No.2775 <br />