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Mar 24 2005 9:20AM McCAMPBELL ANALYTICAL 9257984612 <br />p.2 <br />DHS Certification No. 1644 --Angela Rydelius, Lab Manager <br />110 2nd Avcauc South, #D7, Pacheco, CA 94553-5560 <br />Analytical, <br />McCampbell Analytical, Inca <br />Tole -phone: 925-799-1620 Fax :925-196-1622 <br />J <br />Website: www.mccampbell.com E-mail: main®mccampbell.com <br />Allied Waste Client Project ID: #1733/926900; STP -F- Date Sampled: 03/18/05 <br />04 <br />Date Received: 03/21/05 <br />1145 West Charter Way <br />Client Contact: Brad Bonner Date Extracted: 03/21/05-03/22/05 <br />Stockton, CA 95206 <br />Client P.O.: Date Analyzed: 03/23/05 <br />Gasoline Range (C6 -C12) Volatile Hydrocarbons as Gasoline with BTEX and MTBE* <br />Extraction method: SW1311(ZHETCIP) Analytical methods: SW8021B/8015Cm Work Order 0503346 <br />Lab ID Client ID <br />Matrix <br />Extraction <br />TPH(g) <br />MTBE <br />Benzene <br />Toluene <br />Ethylbcraene <br />Xylenes DF I % SS <br />OOlA i Comp i <br />S <br />ZHETCLP <br />— <br />-- s <br />ND<0.005 <br />0.064 <br />0.021 <br />0.28 2 ! 117 <br />--• <br />-- <br />0.0055 <br />0.076 <br />0.019 <br />002A Comp h2 <br />S 1 <br />ZHETCLP <br />0.25 i 2 113 <br />j <br />I <br />I <br />1 <br />i <br />i <br />I-- <br />' <br />i <br />i <br />t <br />I <br />— <br />i <br />r <br />, <br />Reporting Limit for DF =1; <br />W <br />T -1C <br />N,NA <br />NA <br />NA <br />NA <br />NA NA <br />ND means not detected at or <br />above the repotting limit <br />---- -- - <br />1 S <br />- ------ -- <br />ZHETCLP <br />0.0005 nig; L <br />—___.._ <br />0.05 <br />0.005 <br />0.0005 <br />1)0.0005 <br />0.0005 <br />* water and vapor samples and all TVLP & SPLP extracts are reported in µg(L, soil/studgelsolid samples in pg/kg, wipe samples in µg/wipe, <br />productJoil/non-aqueous liquid samples in mg/L. <br /># cluttered chromatogram; sample peak coelutes with surrogate peak - <br />+The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation: a) <br />unmodified or weakly modified gasoline is significant; b) heavier gasoline range compounds are signifrcant(aged gasoline7); c) lighter gasoline range <br />compounds (the most mobile fraction) are significant; d) gasoline range compounds having broad chromatographic peaks are significant; biologically <br />altered gasoline?; e) TPH pattern that does not appear to be derived from gasoline (stoddard solvent / mineral spirit?),- f) one to a few isolated non -target <br />peaks present-, g) strongly aged gasoline or diesel range compounds are significant; h) lighter than water immiscible sheen/product is present; i) liquid <br />sample that contains greater than –I vo(. % sediment; j) no recognizable pattern; k) TPH pattern that does not appear to be derived from gasoline <br />aviation as). <br />DHS Certification No. 1644 --Angela Rydelius, Lab Manager <br />