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Laboratory Control Spike Recovery <br /> EPA 8260B <br /> APPL ID: 070515W-61391 LCS -112639 APPL Inc. <br /> Batch ID: $82C2-070514BC 4203 West Swift Avenue <br /> Fresno, CA 93722 <br /> Compound Name Spike Level SPK Result SPK% Recovery <br /> ug/L ug/L Recovery Limits <br /> Vinyl Acetate 10.0 13.2 132# 70-130 <br /> Vinyl chloride 10.0 12.1 121 70-141 <br /> Xylenes 30.0 26.8 89.3 70-130 <br /> ----------------------------------------------------------------- - ---------------------------------------------------------------------------------------- <br /> Surrogate: 1,2-Dichloroethane-d4 16.9 17.7 105 70-130 <br /> Surrogate:4-Bromofluorobenzene 18.8 21.0 112 70-130 <br /> Surrogate: Dibromofluoromethane 18.1 19.2 106 70-130 <br /> Surrogate:Toluene-d8 18.5 16.5 89.2 70-130 <br /> --- -------- ------- -------- -------- ------------- ------ --------- ------- --------- <br /> #= Recovery is outside QC limits. <br /> Comments: <br /> — Primary SPK <br /> Quant Method : C82C2.M <br /> Extraction Date: 5/15/2007 <br /> Analysis Date : 5/15/2007 <br /> Instrument: Chico <br /> Run : 0514C22 <br /> Initials: GM <br /> Printed: 5/21/2007 2:25:09 PM <br /> APPL Standard LCS <br /> 17 <br />