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Herst Associates Project: Misc.Samples Reported: 05/23/2007 13:31 <br /> 4630 South Highway 94 North Outer Road Project Number: [none] <br /> North Outer Rd. Project Manager: David Vasbinder <br /> Saint Charles,MO 63304 <br /> Volatile Organic Analysis (EPA Method 8260) <br /> BCL Sample ID: 0705833-02 Client Sample Name: FIELD BLANK @ NORTH STORAGE TANK,5/17/2007 8:45:OOAM,David Vasbinder <br /> Prep Run Instru- QC MB Lab <br /> Constituent Result Units PQL MDL Method Date DatelTime Analyst ment ID Dilution Batch ID Bias Quals <br /> Acrylonitrile ND ug/L 5.0 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> t-Amyl Methyl ether ND ug/L 0.50 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> t-Butyl alcohol ND ug/L 10 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> Carbon disulfide ND ug/L 1.0 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> trans-1,4-Dichloro-2-butene ND ug/L 5.0 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND V11 <br /> Diisopropyl ether ND ug/L 0.50 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> Ethanol ND ug/L 250 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> Ethyl t-butyl ether ND ug/L 0.50 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> 2-Hexanone ND ug/L 20 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> Methyl ethyl ketone ND ug/L 10 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> Methyl iodide ND ug/L 2.0 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND V11 <br /> Methyl isobutyl ketone ND ug/L 10 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> Vinyl acetate ND ug/L 10 EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 ND <br /> 1,2-Dichloroethane-d4(Surrogate) 102 % 76-114 (LCL-UCL) EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 <br /> Toluene-d8(Surrogate) 102 % 88-110 (LCL-UCL) EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 <br /> 4-Bromofluorobenzene(Surrogate) 99.8 % 86-115 (LCL-UCL) EPA-8260 05/18/07 05/18/07 18:00 MWB MS-V9 1 BQE1080 <br /> BC Laboratories The results in this report apply to the samples analyzed in accordance with the chain of custody document.This analytical report must be reproduced in its entirety. <br /> Page 9 of 42 <br />