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:M LABORATORIES, INC. <br /> Herst Associates Project: NCYC Reported: 03/20/2008 12:48 <br /> 4630 South Highway 94 North Outer Road Project Number. [none] <br /> Saint Charles, MO 63304 Project Manager: David Vasbinder <br /> Volatile Organic Analysis (EPA Method260) <br /> BCL Sample ID: 0803475-09 Client Sample Name: Trip Blank, 3/13/2008 12:00:OOAM, David Vasbinder <br /> Prep Run __- Instru- QC MB Lab <br /> Constituent Result Units PQL MDL Method Date Date/Time Anal st ment ID Dilution Batch ID Bias Quals <br /> t-Butyl alcohol <10 uglL 10 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> _----- _._.. — ....... -.. w.. <br /> Carbon disulfide <1.0 ug/L 1.0 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> ....... ... _.. .......... _ _._.......--- ...... <br /> trans-1,4-Dichloro-2-butene <5.0 ug/L 5.0 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> ....... .....------------- .—...._.— - - ----- __._.__. ................._.._ <br /> Diisopropyl ether_ ......... _...... ------- _ _............ _..__ . _-------------- --- ---- <br /> Ethanol <250 ug/L 250 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> _._._.___..._._.—----- — _.— ......._. —..._._......—._. __._._ __.._. --.,... ....._. <br /> Ethyl t-butyl ether <0.50 ug/L 0.50 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> -- _..__ ._....—. — <br /> 2-Hexanone <10 ug/L 10 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> _ _--------- ._..----._._. _...- —__..-. - .. -- <br /> Methyl ethyl ketone <10 ug/L 10 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> ------------..—_- .-------------_. ..—. ... L — .._ —._._._ -- _......- <br /> Methyl iodide <2.0 ug/L 2.0 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> ..............._._. _. .. - -----.._._..... ----- _. <br /> Methyl isobutyl ketone <10 ug/L 10 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> ...... _ _. ...... — _._. <br /> Vinyl acetate <10 ug/L 10 EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 ND <br /> 1,2-Dichioroethane-d4(Surrogate) 104 % 76-114 (LCL-UCL) EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 <br /> --....__�..__......._—.-....-- �... —...............__......,.- .-- ------- <br /> Toluene-d8(Surrogate) 99.3 % 88-110 (LCL-UCL) EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 <br /> - — ..._... _ ......... _ ..... ------- <br /> 4-Bromofluorobenzene(Surrogate) 96.2 % 86-115 (LCL-UCL) EPA-8260 03/18/08 03/19/08 05:34 ANO MS-V4 1 BRC0903 <br /> BC Laboratories The results in this report apply to the samples analyzed in accordance with the chain of custody document. Ais analytical report must he reproduced in!is!entirety. <br /> All results listed in this report are for the exclusive use of the suhnuffing party.BC Laboratmics,Inc.assumes no responsibility for report alteration,separation; detachment or third party interpretation. Page 32 of 38 <br /> 4100 Atlas Court.Bakersfield,CA 93308 ®(661)327-4911 -FAX(661)327-1918 4 www.bclabs.com <br />