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LABORATORIES, INC. Horst Associates Project: NCYC Reported: 03/03/2008 14:50 4630 South Highway 94 North Outer Road Project Number: [none] Saint Charles, MO 63304 Project Manager: David Vasbinder Volatile Organic Analysis (EPA Method260) BCL Sample ID: 0802520-01 Client Sample Name: FB @ Well#2, 2/22/2008 7:29:OOAM Prep Run instru- QC M13 Lab Constituent Result Units PQL MDL Method Date Date/Time Analyst ment lD Dilution Batch iD Bias Quals t-Butyl alcohol NO ug/L 10 8.6 EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO - -......--..._...— .................. _--------- ................. __...- _._.............. - -- -- - Carbon disulfide NO ug/L 1.0 0.40 EPA-8260 02127/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO -- -----.....................- _.W.._. --.._...._..........--------..._._................ trans-l,4-Dichioro-2-butene NO ug/L 5.0 2.0 EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO —. -.......... ---- .... ------. — Diisopropyl ether NO ug/L 0.50 0.18 EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO .._- ------ Ethanol NO ug/L 250 57 EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO _ ...---....._ ...-........ --... _ -----........................_....................._.........,............ ......._....................... ....... ----- _..._....—_._...._..._.... - Ethyl t-butyl ether NO ug/L 0.50 0.22 EPA-8260 02/27/08 02128/08 17:03 MGC MS-V5 1 BRB1714 NO —....---- -.._.._.... - .._..... ..._... - -..._.-..._._....- ---.._.. --------------- ..._............._......_...._...__ 2-Hexanone NO ug/L 10 2.5 EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO ......................_........... ----.._.... - - - .., ---._._.._-.._-.._-.._...-.- --------_.. --—----- Methyl ethyl ketone NO ug/L 10 1.6 EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO ............... ----...............-._......._._........_.....----- ----- -.._........_.........____._.,_............_............ - - Methyl iodide NO ug/L 2.0 0.42 EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO -.—I....... ---..............__.............._....................._......................-----------............... ----------- --------.. -----------................._.._,_ Methyl isobutyl ketone NO ug/L 10 3.4 EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO ----.�..__.....__... —..__......_.._._.__._- -..__.._......_.._.........................._------- - ..._......_---- -_- - ............_.-------------..- -- - Vinyl acetate NO ug/L 10 3.1 EPA-8260 02/27108 02/28/08 17:03 MGC MS-V5 1 BRB1714 NO ..........._ --- ---- - _...._. _ ---------- _ -- ._.__._....._.......---- --- 1,2-Dichloroethane-d4(Surrogate) 103 % 76-114 (LCL-UCL) EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 ,._— --- ---------------- ----.-......_....... . .. -- -._.. . ....... ..-- .........................—-- ---._ - .-. Toluene-d8(Surrogate) 101 % 88 110 (LCL-UCL) EPA-8260 02/27/08 02/28/08 17:03 MGC MS-V5 1 BRB1714 _._.—. -_ -------............................------------------ - ..._.._ _ ---- -._... ------.-.-------._..----------- _._.....,,... _. 4-Bromofluorobenzene(Surrogate) 100 % 86-115 (LCL-UCL) EPA-8260 02/27/08 02/28108 17:03 MGC MS-V5 1 BRB1714 BC Laboratories The results in this report apply to the samples analyzed in accordance with the chain of custody document.This analytical report must be reproduced in its entirety. All results listed in this report are for the exclusive use of the submitting patty.BC Laboratories,Inc.assumes no responsibility for report alteration,separation, detachment or third party interpretation. Page 5 of 35 4100 Atlas Court-Bakersfield,CA 93308-(661)327-4911 -FAX(661)327-191.8•www.bclabs.com