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rli_Laboratories Inc Environmental Testing Laboratory Since 1949 Herst Associates Project: NCYC Reported: 10/07/2009 13:55 4630 South Highway 94 North Outer Road Project Number: Austin Road Saint Charles, MO 63304 Project Manager: Erin Fanning Volatile Organic AnalTA ( A Method 8260) BCL Sample 1D: 0913032-06 Client Sample Name: CYA 1, 10/1/2009 9:25:OOAM,John Regan Prep Run Instru- QC MB Lab Constituent Result Units PQL MIDI.. Method Date Date/Time Analyst ment ID Dilution batch ID Bias Quals t-Butyl alcohol ND ug/L 10 9.2 EPA-8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 ND ---- --. .-------------- Carbon ---_Carbon disulfide ND ug/L 1.0 0.40 EPA-8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 N -- ._....................................... ..................... .- ND trans-l,4-Dichloro-2-butene ND ug/L 5.0 1.4 EPA-8260 10/05/09 10/05109 19:41 MGC MS-V5 1 BSJ0211 .............. ..-................ ............... ---- --- -- ---- ----- .. ......... .._ ..... _ _ Diisopropyl ether ND ug/L 0.50 0.15 EPA-8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 ND -- - --- ---- -- .........._._...-----------.-- - --- Ethanol ND ug/L 250 56 EPA-8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 __...-.__. __._____-__- -- •----.._...----- ............. --......-_...._-_.- ---..--- - - ._-- -._. ............... .........._._..._,. Ethyl t-butyl ether ND ug/L 0.50 0,22 EPA-8260 10/05/09 10/05/09 19:41 MGC MS V5 1 BSJ0211 ND __.._......__ __..... _ _- --.- 2-Hexanone ND ug/l. 10 2.9 EPA-8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 ND ...._....--..._.......................-......................._._......_.........---------- .. -...,....._.....,._.._.,._..._.... _...................._..................... ........._.--_.._ -� Methyl ethyl ketone ND ug/L 10 2.4 EPA-8260 10/05/09 10105/09 19:41 MGC MS-V5 1 BSJ0211 ND . --------- . - ..............--- .._.._..----....__.- --- ---.............._.... - - - -- -_- ._.-.._......................__................................... .._... Methyl iodide ND ug/L 2.0 0.42 EPA-8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 ND . ...._-.__.....__.._._..__.-------- -.. - - - --------- --------------- ---- ---._.....__................-...................-----------...._.. Methyl isobutyl ketone ND ug/L 10 3.4 EPA-8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 ND ................._.,...._... _.._.._..._-..._ . ._....._.....__..........._....... .. ...... ..--- ... . -_- --- - Vinyl acetate ND ug/L 10 2.4 EPA 8260 10/05/09 10/05/09 19.41 MGC MS-V5 1 BSJ0211 ND ----........----- _...__ .....-- _._. ... .....--- ----- - -.__---.. 1,2-Dichloroethane-d4(Surrogate) 99.5 % 76 114 (LCL UCL) EPA 8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 .. ....._. __.._.... .._._._..........._.... ... ................ .......-.-_.............. .... ........................... - Toluene-d8(Surrogate) 98.1 % 88-110 (LCL-UCL) EPA-8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 ... . . -_...._.. - ....... _...._._.._.......--------------------...-_...... --.._-.-__....-- --- - - - -_...-- ----- -- .-._......._._._........ 4-Bromofluorobenzene(Surrogate) 94.2 % 86-115 (LCL-UCL) EPA-8260 10/05/09 10/05/09 19:41 MGC MS-V5 1 BSJ0211 The results in this report apply to the samples analyzed in accordance with the chain of custody document.This analytical report must be reproduced in its entirety. All results listed in this report are for the exclwive use of the submitting;party. BC Laboratories,Inc.assurnes no responsibility for report alteration,separation,delacluitent or third patty interpretation. 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bcfabs.com Page 21 of 44 Certifications: California-ELAP Certification Number 1186; Nevada Administrative Code-NAC-445A