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r r� err r it r r r� r r r r r ris aboratories Inc. ljoil— Environmental Testing Laboratory Since 1949 Herst Associates Project: NCYC Reported: 10/07/2009 13:55 4630 South Highway 94 North Outer Road Project Number: Austin Road Saint Charles, MO 63304 Project Manager: Erin Fanning Volatile Organic Analysis (EPA Method 8260) BCL.Sample ID: 0913032-07 Client Sample Name: CYA 1 DUP, 10/1/2009 9:25:OOAM,John Regan Prep Run Instru- QC MB Lab Constituent Result Units PQL MDL Method Date Date/Time Analyst ment ID Dilution Batch 1D Bias Quals t-Butyl alcohol NO ug/L 10 9.2 EPA-8260 10/05/09 10/05/09 20:09 MGC MS-V5 1 BSJ0211 NO ....... ..... .. _... ._..,.__ ............_. ......................._ ..,.....------ -- NO Carbon disulfide NO ug/L 1.0 0.40 EPA-8260 10/05/09 10/05/09 20:09 MGC MS V5 1 BSJ0211 -.. -....�.._....._...._.......-... -------- .......-_._- - --— ----... ......._.__.._.........................._..................._ _...._ - trans-l,4-Dichloro-2-butene NO ug/L 5.0 1.4 EPA-8260 10/05/09 10/05/09 20:09 MGC MS-V5 1 BSJ0211 D ...... - _.� - - ....- -......_.._ -- ....__ .. _.._.......... .. ........._.._...._.-- - -... Diisopropyl ether NO ug/L 0.50 0.15 EPA-8260 10/05/09 10/05/09 20:09 MGC MS-V5 1 BSJ0211 N I.D ------------------........................... -----........_......-1----------- ---Ethanol NO ug/L 250 56 EPA-8260 10/05/09 10/05/09 20:09 MGC MS-V5 1 BSJ0211 NO -- -- -...... - -------- ---........_......... . .- —.. -......_.__._.,_............... _ -_ - -- ._-.._......................................................... - --- Ethyl t-butyl ether NO ug/L 0.50 0.22 EPA 8260 10/05/09 10/05/09 20:09 MGC MS-V5 1 BSJ0211 ND .._..........._.._.....__...___...-.._..___._ ----- ----.....-._-...._._...._._....-- - -- - - ---- _-_.. _.. .. .._., 2-Hexanone NO ug/L 10 2.9 EPA-8260 10/05/09 10/05/09 20:09 MGC MS-V5 1 BSJ0211 N D _._....._....-.---- ............... -...._ _-_..._. - ._.__....... — - ---...-- - --..................... ...-.......---------- --.... ---- --. _.... Methyl ethyl ketone NO ug/L 10 2.4 EPA-8260 10105109 10/05/09 20:09 MGC MS-V5 1 BSJ0211 NO ----- - ._..... -- ---------------------------........................ Methyl iodide NO ug/L 2.0 0.42 EPA-8260 10/05/09 10105/09 20:09 MGC MS-V5 1 BSJ0211 NO -- ..__.... -_- ... ....... - ----- - ...... _ ..-.. ...... - - ... Methyl isobutyl ketone NO ug/L 10 3.4 EPA 8260 10/05/09 10/05/09 20:09 MGC MS-V5 1 BSJ0211 ND Vinyl acetate ND ug/L 10 2.4 EPA-8260 10/05/09 10/05/09 20:09 MGC M8-V5 1 BSJ0211 NO ---- - ..._ --- - -- -....................... ...... - -- - --- --- _._.. -.....---......,................ -....- --- -- ......---....................._..... 1,2-Dichloroethane-d4(Surrogate) 98.1 % 76-114 (LCL-UCL) EPA-8260 10/05/09 10/05/09 20:09 MGC MS-V5 1 BSJ0211 ........._..-.—..-_----...... _..- _-..._ -._.....__._..•-_— - -...._.._-..._... ...-_-..-_.-- ............................._..._..._..- -_--. _._....... Toluene-d8(Surrogate) 100 % 88-110 (LCL-UCL) EPA-8260 10/05/09 10/05/09 20:09 MGC MS-V5 1 BSJ0211 ..........----- -.-_._... ..._..__ --.-......................_...........--. ---------- ........... --...- ----_..-..._........................................ 4-Bromofluorobenzene(Surrogate) 96.9 % 86-115 (LCL-UCL) EPA-8260 10/05/09 10105/09 20:09 MGC MS-V5 1 BSJ0211 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. All results listed in avis report are for the exclusive use of die subulitiint;party. BC I..aboratories,Inc.assumes no responsibility for report alteration,separation,detachment or third party iliterpretation. 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 wtww.bclabs.com Page 24 of 44 Certifications: California-ELAP Certification Number 1186; Nevada Administrative Code-NAC-445A