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Laboractories, Inc. I Environmental Testing Laboratory Since 1949 Herst Associates Project: NCYC Reported: 10/07/2009 13:55 4630 South Highway 94 North Outer Road Project Number: Austin Road Saint Charles, MC 63304 Project Manager: Erin Fanning Volatile Organic Method 8260) Quality Control Repo - Precision & Accuracy Control Limits Source Source Spike Percent Percent Constituent Batch ID QC Sample Type Sample ID Result Result Added Units RPD Recove RPD Recoveg Lab Qualls Bromodichloromethane BSJ0211 Matrix Spike 0913032-03 ND 24.350 25.000 ug/L 97.4 70-130 Matrix Spike Duplicate 0913032-03 ND 23.440 25.000 ug/L 3.8 93.8 20 70-130 _. --....__ -........-- - ..._ - -- _ .......-- - .............----. ...... - --....... --. --.-__...._.......- -...--._. - Chlorobenzene BSJ0211 Matrix Spike 0913032-03 ND 24.690 25.000 ug/L 98.8 70-130 Matrix Spike Duplicate 0913032-03 ND 26.100 25.000 ug/L 5.6 104 20 70-130 .--_..._.__...... _................. .-._.._._. -- - - -. . ...... __.................._-�_._._..._............_..� -- ...................._.__-_.... ......__.._-. _.......... __...-....... . _.._.._.... - Chloroethane BSJ0211 Matrix Spike 0913032-03 ND 22.890 25.000 ug/L 91.6 70-130 Matrix Spike Duplicate 0913032-03 ND 24.530 25.000 ug/L 6.9 98.1 20--..... 70-130 ..---- - ---------... . . --._....-- 1,4-Dichlorobenzene BSJ0211 Matrix Spike 0913032-03 ND 25.840 25.000 ug/L 103 70-130 Matrix Spike Duplicate 0913032-03 ND 27.610 25.000 ug/L 6.6 110 20 70-130 --...__-----....__.................- ---- ._�. _.......-._.... -_.. .-.-.....--...___ --..._..---..,---- - -- .........- -....... -._....._..._._._.- --- 1,1-Dichloroethane BSJ0211 Matrix Spike 0913032-03 ND 23.960 25.000 ug/L 95.8 70-130 Matrix Spike Duplicate 0913032-03 ND 24.150 25.000 ug/L 0.8 96.6 20 70-130 .. ............. -- -- - -......... __.... ..... .....- .- -- -- --... - ..._................... 1,1-Dichloroethene BSJ0211 Matrix Spike 0913032-03 ND 25.120 25.000 ug/L 100 70-130 Matrix Spike Duplicate 0913032-03 ND 25.900 25.000 ug/L 3.1 104 20 70-130 -........................._-.__.... - ._..__._-_ ---- - �__.-..... - ..........--....-_._._ ......-----.-........_.......... -- - - _ Toluene BSJ0211 Matrix Spike 0913032-03 0.17000 24.860 25.000 ug/L 98.8 70-130 Matrix Spike Duplicate 0913032-03 0.17000 25.290 25.000 ug/L 1.7 100 20 70-130 130 ---- ... .....-_... _...,__. ---- __._........,---- .................----_- ...........-- ....-..____-.._..._._-_.. ......._-- ............... .._...... Trichloroethene BSJO211 Matrix Spike 0913032-03 ND 24.120 25.000 ug/L 96.5 70-130 Matrix Spike Duplicate 0913032-03 ND 24.290 25.000 ug/L 0.7 97.2 20 70-130 - -- - _._....,,. -_.- _...... _..........................._.._� -_ _. ....- ...._ ........- -_._._ _.----- --_-. _ 1,2-Dichloroethane-d4(Surrogate) BSJO211 Matrix Spike 0913032-03 ND 9.5600 10.000 ug/L 95.6 76- 114 Matrix Spike Duplicate 0913032-03 ND 9.4200 10.000 ug/L 94.2 76- 114 -------...._..._...... ....... . --- ----.._.�_.._...._._-_._._.. _............_._._...--- ..._... ---_- . . ..__...- -- -__......_........... - Toluene-d8(Surrogate) BSJ0211 Matrix Spike 0913032-03 ND 9.9700 10.000 ug/L 99.7 88-110 Matrix Spike Duplicate 0913032-03 ND 10.120 10.000 ug/L 101 88-110 ...............---- - - --- ............... ---- -_._._. ....._._....._._._ ........._ _.............__.... .... ----- ...... .-.-.-.._ 4-Bromofluorobenzene(Surrogate) BSJ0211 Matrix Spike 0913032-03 ND 9.7900 10.000 ug/L 97.9 86-115 Matrix Spike Duplicate 0913032-03 ND 9.9900 10.000 ug/L 99.9 86-115 _..- ------ - -------- - ---- . ..- -.._.. .....---- ._.- _ ....._ _ -- ... ----- - Benzene BSJ0219 Matrix Spike 0913003-01 ND 30.020 25.000 ug/L 120 70-130 Matrix Spike Duplicate 0913003-01 ND 26.540 25.000 ug/L 12.3 106 20 70-130 - - - -------.............------_......_._._........__._....._._._. -------.._.........................------_-............-- _.-----------...._-......... -.-_..._ - -...----- - - Bromodic hloromethane BSJ0219 Matrix Spike 0913003-01 ND 26.550 25.000 ug/L 106 70-130 Matrix Spike Duplicate 0913003-01ND 23.990 25.000 ug/L 10.1 96.0 20 70-130 The results in this report apply to the samples anal}-ed in accordance with the chain of custody document.This analytical report must be reproduced in its entirety. All results listed in ibis resort are for the exclusive use of the submitting party. BC Laboratories,Inc.assumes no resporuibility for report alteratiun,separation,detaclnuent or third party interpretation. 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www,bclabs.com Page 32 of 44 Certifications: California-ELAP Certification Number 1186; Nevada Administrative Code-NAC-445A