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M M M MI 950�1 Laboratories Inc. : Environmental Testing Laboratory Since 1949 Herst Associates Project: NCYC Reported: 10/07/2009 13:55 4630 South Highway 94 North Outer Road Project Number: Austin Road Saint Charles, MO 63304 Project Manager: Erin Fanning Volatile organic Analysis (EPA Method 8260) Quality Control Report - Laboratory Control Sample _Control Limits Spike Percent Percent Constituent Batch ID QC Sample ID QCT a Result Level PQL Units Recovery RPD Recovery RPD Lab Quals Benzene BSJ0118 BSJ0118-8S1 LCS 24.490 25.000 0.50 ug/L 98.0 70-130 _-... ..................._._._.........-......----...-..-----------...._-._..._..._- -. --..._..._..._............._.__.... --.......- ..._ . - ._-...__-._-_-_- Bromodichloromethane BSJ0118 BSJO118-BSI LCS 23.970 25.000 0.50 ug/L 95.9 70-130 _ ........... ............... ._._.._.- ..^_.-__- ........._ _.--------- - - . - .. Chlorobenzene BSJ0118 BSJ0118-BS1 LCS 26.190 25.000 0.50 ug/L 105 70130 ...............__..�_-.-_- -�_-.. _. ... _ _... Chloroethane BSJO118 BSJ0118-BS1 LCS 23.870 25.000 0.50 ug/L 95.5 70-130 - -- ....- ------ __._.._._.................... ... . ...........__ ...-- --.. _......_._........._.. _ - __ -- -- .... _-.........._.. _ 1,4-Dichlorobenzene BSJO118 BSJO118-BSI LCS 26.790 25.000 0.50 ug/L 107 70-130 1,1-Dichloroethane BSJ0118 BSJ0118-BSI LCS 24.010 25.000 0.50 ug/L 96.0 70-130 -- -- ---................._..._._.--..__...-._--..----.....----------._...------ - --- -.......... ---- - - ......,_ . _ - 1,1-Dichloroethene BSJO118 BSJ0118-BS1 LCS 25.660 25.000 __----_.. __......_-_---__ug/ ---103 ------- - 70-130. T --------- ......------._..-....-----.......__._- ._...-- - -- - ................... -..._ ---------------------------- Toluene BSJO118 BSJO118-BSI LCS 24.330 25.000 0.50 ug/L 97.3 70-130 ------...-.._. ...._..�-_......_.. .....--...._- -._- -- •.. -._ -_..... ............_. ..- ...-.- ... ............... .... __..........._ _. .... ....................._......... - ... Trichloroethene BSJO118 BSJO118-BSI LCS 28.400 25.000 0.50 ug/L 114 70-130 �.---- - ---- -_-..-.................... ... _ .^ -_-___. -- - - ----- 1,2-Dichloroethane-d4(Surrogate) BSJO118 BSJO118-BSI LCS 9.2400 10.000 ug/L 92.4 76-114 ....._ -- --............................ ---- _ ...__._ --- _ _-_.- ..-..- .. Toluene-d8(Surrogate) BSJO118 BSJ0118-BS1 LCS 10.060 10.000 ug/L 101 88-110 ............---_ ---- - - -- 4-Bromofluorobenzene(Surrogate) BSJO118 BSJO118-BSI LCS 10.280 10.000 ug/L 103 86-115 - - -._._._- _-- -------_ ..._.... ••- ..-_.-. _- -_ _......._ .,..-_-._..-__ .................... ..----------------- Benzene BSJ0211 BSJ0211-BSI LCS 24.970 25-000 0.50 ug/L 99.9 70-130 ._._..... - ......-_.__....._..----.._..-- -- -.-. _._........ ...._-._.- - ---- _ -..._�_-_.._-_...._.. - - --. Bromodichloromethane BSJ0211 BSJ0211-BS1 LCS 23.210 25.000 0.50 ug/L 92.8 70-130 ----._....._ __-..... _........... --_----------------_.......-----------__-_ -..._.--------._.. ----- --................. - -_-.-_.... ....-----.._..---- Chlorobenzene BSJ0211 BSJ0211-BSI LCS 26.140 25.000 0.50 ug/L 105 70-130 .-_...._......._..------- - -................ ..... -...... ... ............ - Chloroethane BSJ0211 BSJ0211-BSI LCS 24.310 25.000 0.50 ug/L 97.2 70-130 - ..... ........ - - --- .----- - .. --- --... _ _.- - ... 1,4-Dichlorobenzene BSJ0211 BSJ0211-BS1 LCS 27.690 25.000 0.50 ug/L 111 70-130 ................... .._.- --.................... _._ _..._.....--------- ---------- -----......_....•._...- - - ---. _ ............_....._. - 1,1-Dichloroethane BSJ0211 BSJ0211-BS1 LCS 24.610 25.000 0.50 ug/L 98.4 70-130 __.. . _..... _..-----......_-_ ----..---- --- _-...... _ ._........_.............. _.._ ..........._..-1."----- . .......- -- - ........,._. ...-.._-__ -- -- 1,1-Dichloroethene BSJ0211 BSJ0211-BSI LCS 26.170 25,000 0.50 ug/L 105 -- 70_130 _.....a........-. ....__...._..- -- --.._..---------------_- -.._ _..... . - ..._ ..__........._.._._-...- _. ... -- Toluene BSJ0211 BSJ0211-BSI LCS 23.560 25.000 0.50 ug/L 94.2 70-130 -................__. -� __._.._.-_.-_ .... .-.._ .....-._- ._...--- .....--_ -- .._---•--.... _.. -------..... _-__-__ .__.. Trichloroethene BSJ0211 BSJ0211-BSI LCS 23.530 25.000 0.50 ug/L 94.1 70-130 ...._....._- __._ ..- �._-- ..... ----- -- - ..._..........._ _--.- .. - _- -. .. -_- ... - -.- ............._-_._- ._. 1,2-Dichloroethane-d4(Surrogate) BSJO211 BSJ0211-BS1 LCS 9.7700 10,000 ug/L 97.7 76-114 -_ __._.------- - - - - .... --.._- -----.._-_-._. ..... - -- ..__ - ----- -_... Toluene-d8(Surrogate) BSJ0211 BSJ0211-BSI LCS 9.7500 10.000 ug/L 97.5 88_110 The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Al results listed in this report are for die exclusive use of the submittinu party. BC Laboratories,Inc.assures no responsibility for report alteration,separation,detaclunent or dried party interpretation. 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bclabs.com Page 34 of 44 Certifications: California-ELAP Certification Number 1186; Nevada Administrative Code-NAC-445A