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as little agitation aspossr'ble to tetlucc potential loss of volatile constituents. Major ions, T73S, <br /> and metals analyses (In non-preserved con ° errs) will be collected next followed by samples to <br /> be collected in preserved containers. Containers will be filled directlyfrom the <br /> disposable bailer, <br /> immediately capped,and placed in a tempt - vnitorpd iced chest. Caution will be used not <br /> to overfill bottles containing a preservaziva, T=Wratzzra will be monitored by placing-a <br /> thermometer in the chest and checking to a that there is*Sufficient ice in the chest to <br /> Maifttain a temperature of approximately 4 degrees Celsius The laboratory WM measure; <br /> docftent, and report the temperature of the container n arrival at the Laboratory., <br /> ratory., <br /> The analytical Iaboratory places a total of 2 ml of nitric acid-in some of the I liter- bottles to <br /> reduce the pH to below 2. On an .annual basis an clUra;preserved bottle will be: filled with <br /> groundwater and-the pH measured in the bottle, It is' ed that the pH will be-below 2: If it <br /> is not the field technician will add nitric acid in mcasured amounts until the pH is below 2. This <br /> added quantity of acid will be placed in all the preserved botdcs.dujing the following <br /> ng monitoring ' <br /> rounds until it is checked again the following-y —:Sample4H--will_be-confirifted:at:the.: <br /> laboratory and recorded. Deviations will be documented and reported by the laboratory. <br /> Samples to be submitted for metals analysis filtered in the fieldr Filtering-FriIl be <br /> performed using an in line fiber mecbanisrn which xses tire- t <br /> pumping PrOc=-of.the-dedicated <br /> pump to draw water through the 4 micron-filter A new filter will be used at each well. The new <br /> filters will haYe a minimum of one filter volume of groundwater pressurized <br /> through tltesn to- <br /> rcduca adsorption effects. The actual filtered-sample.wM not be collected-unto a minimum of <br /> two filter volumes of groundwater has been ugh th_ Mter. For wwelLs witFiout <br /> dedicated pumps, the samples are transferred from the bailer,through a filter <br /> app, pito the <br /> appropriate sample container. The filter apparatus consists of a pressure vesszL a hand-operated <br /> Pressure pump, and a filter Water-from the bailer is placed in the pressure vessel and <br /> enough air pressure(via the hand pump)is applied to forme water through the filer caztddge into <br /> the sample bottles. The pressure vessel is washed in conox, steam cleaned, and rinsed with <br /> deic*cd water between wells. A new filar cartridge is used at eaddh well. <br /> Samples will. be labeled with a unique sample ideatificaiion number, project ideaffication, <br /> number,sample locution, and date and time sampled- Samples will be transported to the contract - <br /> laboratory under strict chain-of-custody procedures_. <br /> 23-4939454011231 OR325 A-9 <br /> July 14,2044 <br /> 2000 KkWdder.iaa <br />