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Matrix Spike Recoveries METALS APPL ID: 081107W-86855 MS- 127627 APPL Inc. 4203 West Swift Avenue Sample ID: AX86855 Fresno, CA 93722 Client ID: GWTF-EFL 1108 Method Compound Name Spike Lvi Matrix Res SPK Res DUP Res SPK% DUP% RPD RPD Recovery Extract Analysis Extraci Analysis OC QC ug/L ug/L ug/L ug/L Recovery Recovery Max Limits Date-Spk Date-Spk Date-Dup Date-Dup Group Sample EPA 6010B Aluminum(Al) (Dissolve 2000 ND 1970 1900 98.5 95.0 3.6 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Antimony(Sb) (Dissoly 250 ND 282 275 113 110 2.5 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08127627 AX86855 EPA 6010B Arsenic(As) (Dissolved 250 5.1 259 252 102 98.8 2.7 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Barium(Ba)(Dissolved) 250 301 546 532 98.0 92.4 2.6 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Beryllium(Be) (Dissolve 50.0 ND 50.5 49.1 101 98.2 2.8 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Boron(B)(Dissolved) 250 315 549 536 93.6 88.4 2.4 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Cadmium(Cd)(Dissoly 50.0 ND 48.5 47.3 97.0 94.6 2.5 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Calcium(Ca)(Dissolve 25000 97400 119000 116000 86.4 74.4# 2.6 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 60106 Chromium (Cr)(Dissoly 250 ND 260 253 104 101 2.7 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 w PA 6010B Cobalt(Co)(Dissolved) 250 ND 256 250 102 100 2.4 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Copper(Cu) (Dissolved 250 6.0 253 247 98.8 96.4 2.4 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 60108 Iron (Fe)(Dissolved) 1000 ND 983 954 98.3 95.4 3.0 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Lead(Pb) (Dissolved) 250 ND 242 236 96.8 94.4 2.5 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Magnesium(Mg) (Disso 25000 49900 73000 71100 92.4 84.8 2.6 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 60108 Manganese(Mn)(Disso 250 809 1060 1030 100 88.4 2.9 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Nickel (Ni) (Dissolved) 250 ND 237 232 94.8 92.8 2.1 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Potassium(K)(Dissolve 5000 7470 12200 11900 94.6 88.6 2.5 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 60108 Selenium(Se)(Dissoly 250 ND 225 224 90.0 89.6 0.5 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Silver(Ag) (Dissolved) 100.0 ND 102 99.3 102 99.3 2.7 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Sodium (Na) (Dissolved 25000 53100 76400 74700 93.2 86.4 2.3 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Thallium (TI)(Dissolved 250 ND 238 234 95.2 93.6 1.7 20 80-120 11/W08 11/10/08 11/7/08 11/10/08 127627 AX86855 EPA 6010B Vanadium(V)(Dissolve 250 21.0 283 276 105 102 2.5 20 80-120 11/7/08 11/10/08 11/7/08 11/10/08 127627 AX86855 #= Recovery is outside QC limits. Comments: Printed., 11113108 3:55:26 PM APPL MSD SCH