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Quality Control Data <br /> Client: Republic Services Inc TestAmerica Job ID:480-3228-1 <br /> ' Project/Site:Austin Road Landfill-NCYC <br /> Method: 82608 -Volatile Organic Compounds(GC/MS)(Continued) <br /> ' Lab Sample ID: MB 480-10707/5 Client Sample ID: MB 480-10707/5 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 10707 <br /> ' MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> trans-1,3-Dichloropropene NO 1.0 0.37 ug/L 04/05/111229 1 <br /> trans-1,4-Dichloro-2-butene NO 5.0 2.1 ug/L 04/05/1112:29 1 <br /> Trichloroethene NO 1.0 0.46 ug/L 04/05/1112:29 1 <br /> Trichlorofluoromethane NO 1.0 0.88 ug/L 04/05/1112:29 1 <br /> Vinyl acetate NO 5.0 0.85 ug/L 04/05/11 12:29 1 <br /> Vinyl chloride NO 1.0 0.90 ug/L 04/05/11 12:29 1 • <br /> Xylenes,Total NO 2.0 0.66 ug/L 04/05/11 12:29 1 <br /> MB MB <br /> ' Tentatively Identified Compound Est.Result Qualifier Unit D RT CAS No. Prepared Analyzed Dil Fac <br /> Ethanol TIC NO ug/L 64-17-5 0410511-1 12:21 12:29 1 <br /> MB MB <br /> ' Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> 1,2-Dichloroethane-d4(Surr) 104 66-137 04/05/11 12:29 1 <br /> 4-Bromotluorohenzene(Surr) 90 73-120 04/05/11 12:29 1 <br /> Toluene-d8(Surr) 103 71-126 04/05/11 12:29 1 <br /> ' Lab Sample ID: LCS 480-10707/4 Client Sample ID: LCS 480-10707/4 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 10707 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> 1,1-Dichloroethane 25.0 25.8 ug/L 103 71-129 <br /> 1,1-Dichloroethene 25.0 19.3 ug/L 77 65-138 <br /> 1,2-Dichlorobenzene 25.0 25.5 ug/L 102 77-120 <br /> 1,2-Dichloroethane 25.0 24.2 ug/L 97 75-127 <br /> Benzene 25.0 24.4 ug/L 97 71-124 <br /> Chlorobenzene 25.0 23.2 ug/L 93 72-120 <br /> cis-1,2-Dichloroethene 25.0 24.1 ug/L 96 74-124 <br /> Ethylbenzene 25.0 23.9 ug/L 96 77-123 <br /> Methyl tert-butyl ether 25.0 22.3 ug/L 89 64-127 <br /> Tetrachloroethene 25.0 23.7 ug/L 95 74-122 <br /> Toluene 25.0 23.7 ug/L 95 70-122 <br /> trans-1,2-Dichloroethene 25.0 24.1 ug/L 96 73-127 <br /> Trichloroethene 25.0 23.9 ug/L 96 74-123 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichloroethane-d4(Surr) 103 66-137 <br /> 4-Bromotluorobenzene(Surr) 90 73-120 <br /> Toluene-d8(Surr) 102 71-126 <br /> r <br /> TestAmerica Buffalo <br /> ' Page 14 of 21 04/19/2011 <br />