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September 6, 2011 Lab ID : STK1137299 <br />Forward Inc. Customer : 3-8692 <br />Quality Control - Organic <br />Constituent <br />Method <br />Date/1D <br />Type <br />Units <br />Code, <br />QC DASA <br />DQO <br />Note <br />Organic <br />Vinyl Acetate <br />624 <br />MS <br />ug/L <br />40.00 <br />34.7% <br />27-197 <br />(SP 1108444-002) <br />MSD <br />ug/L <br />40.00 <br />50.4% <br />27-197 <br />MSRPD <br />ug/L <br />10.00 <br />6.3 <br />:5100. <br />624 <br />08/26/11:212696VRG <br />CCV <br />ug/L <br />40.00 <br />67.5% <br />10-150 <br />Vinyl Chloride <br />624 <br />08/25/11:209513VRG <br />Blank <br />ug/L <br />ND <br /><0.5 <br />MS <br />ug/1- <br />10.00 <br />111 % <br />5-283 <br />(SP 1108444-002) <br />MSD <br />ug/L <br />10.00 <br />143% <br />5-283 <br />MSRPD <br />a <br />10.00 <br />1 25.2% <br />515.6 <br />435 <br />624 <br />08/26/11:212696VRG <br />CCV <br />ugfL <br />10.00 <br />74.0% <br />4-196 <br />Xylenes m,p <br />624 <br />08125/11:209513VRO <br />Blank <br />ug/L <br />ND <br /><1.0 <br />MS <br />ug/L <br />20.00 <br />202% <br />62-137 <br />435 <br />(SP 1108444-002) <br />MSD <br />ug/L <br />20.00 <br />185 % <br />62-137 <br />435 <br />MSRPD <br />HVL <br />10.00 <br />9.0% <br />:30.0 <br />624 <br />08/26/11:212696VRG <br />CCV <br />ugIL <br />20.00 <br />125% <br />50-150 <br />Xylenes o <br />624 <br />08/25/11:209513VRG <br />Blank <br />ug/L <br />ND <br /><0.5 <br />MS <br />ug/L <br />10.00 <br />154% <br />65-130 <br />435 <br />(SP 1108444-002) <br />MSD <br />ugfL <br />10.00 <br />145% <br />65-130 <br />435 <br />MSRPD <br />10.00 <br />6.1% <br />511.5 <br />624 <br />08/26/11:212696VRG <br />CCV <br />-ug/L <br />ug/L <br />10.00 <br />102% <br />50-150 <br />PH -Gas <br />80150 <br />08/25/11:209408ACC <br />Blank <br />tng/1. <br />ND <br /><0.05 <br />MS <br />mg/L <br />5.000 <br />110% <br />79-123 <br />(SP 1108388-001) <br />MSD <br />1119/1- <br />5.000 <br />106% <br />79-123 <br />MSRPD I <br />nt <br />5.000 1 <br />4.3% <br />:25.5 <br />Crude Oil <br />8015M <br />08/25/11:209407ACC <br />Blank <br />111 <br />ND <br /><0.5 <br />DIESEL#2 <br />8015M <br />08/26111:212477ACC <br />CCV <br />ntgfL <br />1000 <br />105% <br />85-115 <br />CCV <br />nt <br />1000 <br />110% <br />85-1I5 <br />Gasoline <br />8015M <br />08/25/11:212508ACC <br />CCV <br />Ingfi, <br />5.000 <br />109% <br />85-115 <br />CCV <br />Ill <br />10.00 <br />89.0% <br />85-115 <br />Heavy Oil <br />8015M <br />08/25/11:209407ACC <br />Blank <br />Itt <br />ND <br /><2 <br />8015M <br />08/26/11:212477ACC <br />CCV <br />ntg/L <br />1000 <br />99.0% <br />85-115 <br />CCV <br />m <br />1000 <br />96.1% <br />85-115 <br />Jet Fuel <br />8015M <br />08125/11:209407ACC <br />Blank <br />In <br />ND <br /><0.5 <br />Kerosene <br />8015M <br />08/25/11:209407ACC <br />Blank <br />mg/L <br />ND <br /><2 <br />Mineral Spirits <br />8015M <br />08/25/11:209407ACC <br />Blank <br />in <br />ND <br /><0.5 <br />H -Diesel <br />8015M <br />08/25/11:209407ACC <br />Blank <br />mg/L <br />ND <br /><0.5 <br />LCs <br />mg/L <br />26.32 <br />103% <br />47-144 <br />MS <br />mg/L <br />26.32 <br />101% <br />47-I50 <br />(STK1137376-001) <br />MSD <br />tng/L <br />26.32 <br />106% <br />47-150 <br />MSRPD <br />ttt <br />0.000 <br />5.1% <br />:21.2 <br />Definition <br />CCV : Continuing Calibration Verification - Analyzed to verify the instrument calibration is within criteria. <br />Blank : Method Blank - Prepared to verify that the preparation process is not contributing contamination to the samples. <br />LCS : Laboratory Control Standard/Sanlple - Prepared to verify that the preparation process is not affecting analyte recovery. <br />MS : Matrix Spikes - A random sample is spiked with a known amount of analyte. The recoveries are an indication of !tow that sample <br />matrix affects analyte recovery. <br />MSD : Matrix Spike Duplicate of NIS/MSD pair - A random sample duplicate is spiked with a known amount of analyted. The recoveries <br />are an indication of how that sample matrix a€fects analyte recovery. <br />BS : Blank Spikes - A blank is spiked with a known amount of analyte. Tt is prepared to verify that the preparation process is not <br />affecting analyte recovery. <br />BSD : Blank Spike Duplicate of BS/BSD pair - A blank duplicate is spiked with a known amount of analyte. It is prepared to verify that <br />the preparation process is not affecting analyte recovery. <br />MSRPD : MS/MSD Relative Percent Difference (RPD) - The MS relative percent difference is an indication of precision for the preparation <br />and analysis. <br />BSRPD : BS/BSD Relative Percent Difference (RPD) - The BS relative percent difference is an indication of precision for the preparation. <br />and analysis. <br />Page 13 of 14 <br />