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April 17, 2013 Lab ID <br />San Joaquin County PWD -Solid Waste Div. Customer <br />Quality Control - Organic <br />STK1332913 <br />3-2956 <br />Constituent <br />Method <br />Date/ID <br />Type <br />Units <br />Cone. <br />QC Data <br />DQO <br />Note <br />rganic <br />crolein <br />5030B <br />04/15/13:204052SBL <br />BSD <br />ug/L <br />200.0 <br />13.2% <br />8-101 <br />BSRPD <br />ug <br />25.00 <br />13 <br /><50 <br />Acrylonitrile <br />5030B <br />04/08/13:203800SBL <br />Blank <br />ug/L <br />ND <br /><50 <br />LCS <br />ug/L <br />200.0 <br />150% <br />0-877 <br />MS <br />ug/L <br />200.0 <br />85.5% <br />0-1 <br />435 <br />(SP 1303167-001) <br />MSD <br />ug/L <br />200.0 <br />77.2% <br />0-1 <br />435 <br />MSRPD <br />ug/L <br />25.00 <br />16 <br />1550 <br />Ally] Chloride <br />5030B <br />04/08/13:203800SBL <br />Blank <br />ug/L <br />ND <br /><10 <br />LCS <br />ug/L <br />20.00 <br />43.4% <br />23-236 <br />MS <br />ug/L. <br />20.00 <br />70.0% <br />23-236 <br />(SP 1303167-001) <br />MSD <br />ug/L <br />20.00 <br />61.2% <br />23-236 <br />MSRPD <br />uo/L <br />25.00 <br />1.8 <br />510 <br />Benzene <br />5030B <br />04/09/13:203800SBL <br />Blank <br />ug/L <br />ND <br /><0.5 <br />LCS <br />ug/L <br />25.00 <br />88.5 % <br />77-116 <br />MS <br />ug/L <br />25.00 <br />123% <br />12-174 <br />(SP 1303167-001)' <br />MSD <br />ug/L <br />25.00 <br />122% <br />12-174 <br />MSRPD <br />U. <br />25.00 <br />1.0% <br />524 <br />romobenzene <br />5030B <br />04/08/13:203800SBL <br />Blank <br />ug/L <br />ND <br /><0.5 <br />LCS <br />ug/L <br />25.00 <br />91.6% <br />56-141 <br />MS <br />ug/L <br />25.00 <br />119% <br />4-178 <br />(SP 1303167-001) <br />MSD <br />ug/L <br />25.00 <br />122% <br />4-178 <br />MSRPD <br />ug/L <br />25.00 <br />2.0% <br />529 <br />romochloromethane <br />5030B <br />04/08/13:203800SBL <br />Blank <br />ug/L <br />ND <br /><1 <br />LCS <br />ug/L <br />25.00 <br />86.3% <br />79-119 <br />MS <br />ug/L <br />25.00 <br />107% <br />12-164 <br />(SP 1303167-001) <br />MSD <br />ng/L <br />25.00 <br />104% <br />12-164 <br />MSRPD <br />ug/L <br />25.00 <br />2.4% <br />528 <br />romodichloromethane <br />5030B <br />04/08/13:203800SBL <br />Blank <br />ug/L <br />ND <br /><0.5 <br />LCS <br />ug/L <br />25.00 <br />82.3% <br />63-152 <br />MS <br />ug/L <br />25.00 <br />106% <br />7-181 <br />(SP 1303167-001) <br />MSD <br />ug/L <br />25.00 <br />95.8% <br />7-181 <br />MSRPD <br />ug <br />25.00 <br />10.4% <br />525 <br />romoform <br />5030B <br />04/09113:203800SBL <br />Blank <br />U. <br />ND <br />Q <br />LCS <br />ug/L <br />25.00 <br />100% <br />49-165 <br />MS <br />ug/L. <br />25.00 <br />125% <br />2-170 <br />(SP 1303167-001) <br />MSD <br />ug/L <br />25.00 <br />106 % <br />2-170 <br />MSRPD <br />ug /L <br />25.00 <br />16.8% <br />532 <br />Bromomethane (Methyl Bromide) <br />5030B <br />04/09/13:203800SBL <br />Blank <br />ug/L <br />ND <br /><1 <br />LCS <br />ug/L <br />25.00 <br />95.7% <br />14-238 <br />MS <br />ug/L <br />25.00 <br />127% <br />28-269 <br />(SP 1303167-001) <br />MSD <br />ug/L <br />25.00 <br />125% <br />28-269 <br />MSRPD <br />u_ -/L <br />1 25.00 <br />1.6% <br />533 <br />Carbon Disulfide <br />5030B <br />04/09/13:203800SBL <br />Blank <br />ug/L <br />ND <br /><10 <br />LCS <br />ug/L <br />40.00 <br />76.1% <br />3-148 <br />MS <br />ug/L <br />40.00 <br />97.9% <br />22-143 <br />(SP 1303167-001) <br />MSD <br />ug/L <br />40.00 <br />83.8% <br />22-143 <br />MSRPD <br />ug/L <br />25.00 <br />5.6 <br />510 <br />Carbon Tetrachloride <br />5030B <br />04/08/13:2038000L <br />Blank <br />ug/L <br />ND <br /><1 <br />LCS <br />ug/L. <br />25.00 <br />89.1.% <br />26-203 <br />MS <br />ug/L <br />25.00 <br />146% <br />0-230 <br />(SP 1303167-001) <br />MSD <br />ug/L <br />25.00 <br />132% <br />0-230 <br />MSRPD <br />ng/L <br />25.00 <br />10.3% <br />524 <br />hlorobenzene <br />5030B <br />04108/13:203800SBL <br />Blank <br />ug/L <br />ND <br /><0.5 <br />1 <br />LCS <br />ug/l,25.00 <br />88.I % <br />62-130 <br />Page 14 of 21 <br />n <br />C <br />