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transportation was required. Following desorption with carbon disulfide, <br />analyses were preformed by GC/MS. Analysis of on archived reserve samples <br />nearly a year later produced the some characteristic pattern of <br />chromatographic peaks as had been noted when the samples were first <br />analyzed. This method of archiving samples could be useful in connection <br />with many projects. <br />In 1982 Dr. Mary Havlicek examined glass bottle samples taken in the <br />vicinity of on oil refinery for trace organics. In this case, a packed <br />column was used to separate the components of this complex mixture prior <br />to analysis by GC/MS. Glass sampling bottles are generally not <br />recommended for low-level analyses due to problems associated with leakage <br />and adsorption to the container walls. Since the project in question <br />involved levels approaching those associated with fire hazard, the choice <br />of sampling containers was quite appropriate. <br />Dr. Larry Hilpert, the newest member of the CCAS project team has <br />devoted several years to the analysis of trace organics in air pollution <br />samples. Included among this work was the development of a certified <br />reference moteral for the National Bureau of Standards. Dr. Hilpert has <br />10 years of work experience with the National Bureau of Standards where he <br />has participated in methods development using GC/MS and HPLC. He has more <br />than 10 publications to his credit and is expected to provide major inputs <br />to projects of this type. <br />QUALITY ASSURANCE <br />Quality assurance at CCAS serves two important functions. The first <br />function is the establishment of quality control activities relating to <br />sample collection, siting of sampling stations, analytical protocols and <br />data validation. The second function is the provision of such data <br />quality information as precision accuracy and completeness. <br />The sampling equipment intended for use on site consists of <br />electropolished stainless steel canisters, the sampling manifolds <br />described earlier in the text and presented in figures 2 and 3, Teflon and <br />stainless steel pumps and three meteorological monitoring stations. <br />Canisters and manifolds through which samples are to be passed are <br />leak tested before being brought into the field. Timers, pumps etc. are <br />similarly inspected to verify that they are in good operating condition. <br />Prior to removal of a sample from the sampling manifold, pressure is <br />recorded in the field sampling record book. Meteorological conditions are <br />noted. The time at which sample collection ceased is recorded as is the <br />actual time of sample pickup. The samplers initials and can number are <br />also entered in the field notebook. While the can and the sampler are <br />still at the sampling station, the location is marked on the site map <br />