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u <br />I <br />L <br />0 <br />L <br />r, <br />f'. <br />u <br />sampling forvolatile organics. These bottles are filled completely to prevent air from remaining in the <br />bottle. A positive meniscus forms when the bottle is completely full. A convex Teflon septum is <br />placed over the positive meniscus to eliminate air. After the bottle is capped, it is inverted and tapped <br />to verify that it contains no air bubbles. <br />Dissolved Metals <br />To determine dissolved concentrations of metals, appropriate field filtration techniques are used. <br />When using a Teflon bailer, the sample is filtered by emptying the contents of the bailer into a <br />pressure transfer vessel. A disposable 0.45 -micron acrylic copolymer filter is threaded onto the <br />transfer vessel at the discharge point and the vessel is sealed. Pressure is applied to the vessel <br />with a hand pump and the filtrate is directed into the appropriate containers. Each filter is used <br />once and discarded. <br />When using a bladder pump to collect samples for dissolved constituents, the sample is filtered by <br />attaching a disposable 0.45 -micron acrylic copolymer filter directly to the pump effluent line with <br />a pressure fitting. As the pump cycles, the effluent is pressured through the filter and directed into <br />the appropriate containers. Each filter is used once and discarded. <br />Spring (or Surface Wafer) Sampling <br />If sufficient flow is observed, spring (or surface. water) samples are collected with a dipper consistent <br />with the procedures listed in Section 9 of "Test Methods for Evaluating Solid Waste: <br />Physical/Clnemicai Methods," SW -846, 3rd edition, November 1986. If low -flow conditions are <br />encountered, a stainless steel scoop is used to collect samples. The flat bottom of the scoop is pressed <br />against the bank and the water will flow with little disturbance into the scoop. Samples collected with <br />a dipper or scoop are transferred into the appropriate sample containers. Spring (or surface water) <br />samples are filtered as required. <br />Leachate Sampling <br />If leachate sampling and analysis is required, samples are collected after purging approximately <br />one casing volume using a Teflon bailer. Leachate samples are filtered as required and transferred <br />into the appropriate containers. <br />Lysimeter Sampling <br />If lysirneter sampling and analysis is required, a vacuum is applied to the lysinieter only if an <br />electrical conductivity monitor indicates that the soil -moisture content and soil suction are adequate <br />for attempting to colledt a sample. Vacuum and pressure is alternately applied to lysimeter over a <br />72 -hour period to achieve the sample volume required for analysis. If sufficient sample volume is not <br />Groundwater Monitoring A-4 Department of Public Works/Solid Waste <br />County of San Joaquin <br />