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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McC,AMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccamobell com E-mail mam@mccampbell corn <br /> i <br /> Advanced GeoEnviromnental Client Project ID Waterloo Food&Fuel Date Sarnpled 08/10/01 <br /> 837 Shaw Road Date Received 08/15/01 <br /> IStockton, CA 95215 Client Contact Bill Little Date Extracted 08/16/01 <br /> Client P 4 Date Analyzed 08/16/01 <br /> ISeven Oxygenated Volatile Organics By GC/MS <br /> EPA method$260 modified <br /> Lab ID 74743 74744 74745 <br /> MWI/ MW3/ MW4/ Reporting Limit <br /> Client ID 081001 081001 081001 <br /> Matrix W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DiPE) ND<100 ND<1000 ND<2500 50 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND<100 ND<1000 ND<2500 50 10 <br /> Methyl tert-Butyl Ether(MTBE) 4300 52,000 170,000 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<100 ND<1000 ND<2500 50 10 <br /> tert-Butanol ND<500 ND<5000 ND<13,000 25 50 <br /> Methanol ND<50,000 ND<500,000 ND<1300,000 2500 500 <br /> Ethanol ND<5000 ND<50,000 ND<130,000 250 50 <br /> Surrogate Recoveries(%) <br /> IDibromotlucromethane 106 102 103 <br /> Comments i <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts to ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than N5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644Edward Hamilton,Lab Director <br />