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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//www mccamnbell com E-mail main@mccampbell cam <br /> • <br /> Advanced GeoEnviromnental Client Project LD Waterloo Food&Fuel Date Sampled 04/27/01 <br /> 837 Shaw Road Date Received 04/27/01 <br />' Stockton, CA 95215 Client Contact Bill Little Date Extracted 04/30-05/01101 <br /> Client P O Date Analyzed 04/30-05/01/01 <br />' EPA method 8260 modified Seven Oxygenated Volatile Organics By GC/MS <br />' Lab ID 66329 56330 66331 66332 <br /> MWI / MW2/ MW3/ MW4/ Reporting Limit <br /> tlD 042601 042601 042601 042601 <br /> Matrix W W W W S W <br /> Compound Concentration* <br /> ug/kg ug/L <br />' Di-isopropyl Ether(D1PE) ND<I30 ND<5000 ND<2500 ND<5000 50 1 0 <br />' Ethyl tert-Butyl Ether(ETBF) ND<130 ND<5000 ND<2500 1ND<25,00025 <br /> 10 <br /> Methyl tert-Butyl Ether(MTBE) 4800 180,000 79,000 10 <br /> 1 <br /> tert-Amyl Methyl Ether(TAME) ND<130 ND<5000 ND<2500 10 <br />' tert-Butanol ND<650 ND<25,000 ND<13,000 50 <br />' Methanol ND<65,000 ND<2500,000 ND<1300,000 ND<25000 1000 500 <br /> Ethanol ND<6500 ND<250,000 ND<130,000 ND<250,000 250 50 <br /> Surrogate Recoveries(%) <br />' Dibromofluoromethane 116 102 113 1 l 1 <br /> Comments h h <br /> s water samples are reported in ug/L,soil and sludge samples in uglkg,wipes to ug/wipe and all TCLP/STLC/SPLP extracts to ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water imnusctble sheen is present (t)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 <br /> Edward Hamilton,Lab Director <br /> I <br />