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110 2nd Avenue South,#D7,Pachcoo,CA 94553-5560 <br /> 4 MCCAMPBELL ANALYTICAL INC 'Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccam bell com E-mail rnatn@rnccampbell corn <br /> Advanced GeoEnvxroitsnental Client Project M Waterloo Food&Fuel <br /> Date Sanded 10/31-11f02l02 <br /> Date Received 11106101 <br /> 837 Shaw Road <br /> Stockton,CA 95215 Client Contact Bill Little Date Extracted 11/08-11/12/02 <br /> Client P O Date Analyzed 11/08-11/12/01 <br /> Seven Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br /> Lab 1D 82774 82775 82776 82777 <br /> Reporting Limit <br /> Client ID MW6E/ MW7A/ 1V1W7E/ MW7C/ <br /> 110101 110101 110201 110201 <br /> Matrix W W W W S W <br /> Compound Concentration* ung cg/L. <br /> Dt-isopropyl Ether(DIPF) ND ND<50 ND ND 50 30 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND<50 ND ND 50 1 0 <br /> Methyl tent-Butyl Ether(MTBE) ND 1400 :9:740 rND <br /> 5 o 10 <br /> tent-Amyl Methyl Ether(TAME) ND ND<50 NDso 1 0 <br /> tent-Butanol ND ND<250 ND ND 25 50 <br /> Methanol ND ND<25,000 ND ND 2500 504 <br /> Ethanol ND ND<2500 ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dtbromotluoromethane 104 98 102 103 <br /> Comments i <br /> *water samples are reported in ug/L,soil and sludge samples in uglkg,wipes in ug/wipe and all TCLP!S'TLC 1 SPLP extracts to ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysts <br /> (h)lighter than water immiscible sheen is present,(t)liquid sample that contains greater than M5 vol %sediment C7)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hanulton, Lala Director <br />