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[10 2nd Avenue South,#D7,Pacheco,CA 9.4553-5560 <br /> McCAMPBELL ANALYTICAL INC 'Telephone 925-798-1620 Fax 925-798-1622 <br /> h /Iwww mccam bell com E-mail main@tnecampbell corn <br /> Date Sampled 10/31-11/02101 <br /> Advanced GeoEnvironrnental Client Project ID Waterloo Food&Fuel <br /> 937 Shaw Road Date Received 11/06/01 <br /> Stockton, CA 95215 Client Contact Bill Little Date Extracted 11/08-11/12101 <br /> Client P 0 Date Analyzed 11/08-11/12/01 <br /> Seven Oxygenated Volatile Organtes By GUMS <br /> EPA method 8260 modified <br /> Lab ID 82782 82783 82784 <br /> Reporting Limit <br /> Client ID MW8C/ MWSD! MWBEI <br /> 110201 110201 110201 <br /> Matrix W W W W - <br /> Compound Concentration* ug/kg uWL <br /> Dt-isopropyl Ether(MPE) ND ND ND 5 0 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND 5 0 t 0 <br /> Methyl tent-Butyl Ether(MTBE) ND ND ND 5 0 1 0 <br /> tert-Amyl Methyl Ether JAME) ND ND ND 50 1 0 <br /> Cert-Butane ND ND ND 25 50 <br /> Methanol ND ND ND 2500 500 <br /> Ethanol ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Drbromotluoromethane 107 105 105 <br /> Comments <br /> "water samples are reported in ug/L,soil and sludge samples in ulS,wt es in u 1 i eand all TCLP STLC!SPLP extacts m ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />