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04/08/2002 14 46 2094671118 AGE STCCKTON PAGE 04 <br /> 110 21nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> • cCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htti5//www mccam6elf ncom E-mail matn@rnecaMbell coin <br /> Advanc ed Geolrrvirommental Chert protect lD Waterloo Food/,Fuel Date Sampled 10/25/01 <br /> 837 Shaw Road Date Received 10/26/01 <br /> Stockto ,CA 95215 Client Contact Bill Little Date Extracted 11/01/01 <br /> Client F 0 Date Analyzed 11/01/01 <br /> EPA met ad 8250 Volatile Organics By GC/MS <br /> Lab ID 82063 <br /> Client 1D DW-1 <br /> Matrix W <br /> Compou d Cosieentration" P;��S' <br /> * Reportlna Limit <br /> Compound Caracentratton <br /> W 5 <br /> Arcelone ND so 25 trans-l,3-Dichloropropene ND 10 5 0 <br /> $enzcnc , NJ) 10 50 Ethylene dtbrotnide ND 1 0 5 0 <br /> WBronzone ND 1 0 5 0 Ethylbenzene ND 1 0 5 0 <br /> oromethane ND i d 5 0 HexachlorobutadteneND 50 25loromethane ND 1 0 50 Jodomethane iT 1 0 5 4 ND 10 50 Jsopropylbenzene ND 10 50 <br /> ane0 5Q p-Isopropyl toluene ND 10 50 <br /> mane ND 10 5 0 Methyl butyl ketone ND 10 56 <br /> benzene ND 1 0 5 0 Methylene Chloride` ND 10 50 <br /> benzene ND 10 50– Methyl ethyl ketone ND —To--- 10 <br /> . Carbon D sulfide ND 10 50 Methyl isobutyl ketone 7 FNJJ 1 0 S O <br /> Carbon T trachlonde ND 10 5o Methyl Cert-Butyl Ether(MTI )Z) -- 10 5 0 <br /> Chloro zene ND 10 50 Naphthalene ND 1 0 50 <br /> chloroctl#ne ND l 0 50 n Propyl benzene ND 1 0 50 <br /> 2-chlomclttlyl Vinyl Ether° ND 10 50 Styrene ND 1 0 50 <br /> Chlorofo NO 1 0 5 0 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chlorom have Nil l 0 5 0 1,1,2,2-Tetrach oroethane ND 1-0 50 <br /> 2-Chlorot luene ND 1 0 50 Tetmchloroethene ND 1 0 5 0 <br /> 4- hlorot ]uene N13 10 50 r1,21,4 <br /> ene ND 1 0 50 <br /> 17ibromo larometltanc NP 10 50 3-Tnchlorobenzcne ND 50 25 <br /> 1,2-Dibro 0-3 chloroprapane ND 20 10 -Tnchlorobenzene ND 50 25 <br /> Dlbromo thane N]7 ] 0 5 0 -Trichloroethane ND XO S0 <br /> 1,2-Diehl robenzene ND 10 5 0 -Trichloroethane ND 1 0 50 <br /> 1,3-Dtcltl robenzene ND 1 0 5 0 Trichlarvetbene ND —10 =0 <br /> bi robenzene ND 1 0 5 0 Trichlorofluoromethane ND to 5 0 <br /> jhlary itluommetltane ND —10 5 0 1,2,3-TnchloropropaneND 1 0 5 0 <br /> 1,1-Dtc111 roethme ND 10 5 0 1,2,4-Tnmethylbenzene ND l 0 .50 <br /> 1,2-Diehl methane ND 10 50 1,3,5-Trimethylbenzcne ND 10 50 <br /> 1,1-Diehl roethme ND --1-0—--5--0— Vinyl Acetate "' ND —FO— 25 <br /> cis-1,2 hloroethene ND IQ 5 0 vinyl Chloride ' ND —F-0– 5 0 <br /> trans 1,2 tchloroethene Nr) 1 0 5 0 Nylenes,total ND 1 0 5 0 <br /> 1,2 Dicltl ropropane ND i 0 5 0 Comments <br /> 1,3-Diehl ropropane ND 1 0 S 0 Surrogate Ittecoveric$ <br /> 2,2-Dtch1 ropropane ND 1 0 5 0 Dtbrornofluoromethane 107 <br /> ]IJ-Diehl ropropene ND 10 5 0 Toluene-d8 103 <br /> c3s-1,3-D hlor ropene ND 10 5 0 4$romoflu.r.benzene 98 <br /> 'water aoi vapor samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in u8/wipe and all TCLP/SPLP extracts m u8/L <br /> ND mean not detected above the repotting limit NIA Means analyte not applicable to this analysts <br /> {b)2•pto anone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2 hexanone, (e) dichloromethane, (t) 2-butanone, (8) 4.methyl-2- <br /> pentanoi or tsopropylacctone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than �5 vol % <br /> scdtm(nt, 0) sample diluted due to high oiganic contml, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroeth ne,(o)dimethylberizenes <br /> AHS eztification No 1644 E waird Hamilton,Lab Director <br />