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Quantitation Report (QT Reviewed) <br /> 1 <br /> Data File I \MSDCHEM\1\DATA\051603\05160347 D Vial 20 <br /> Acq On 17 May 2003 7 06 am Operator EL <br /> Sample MME0164-01@BLAES ENV (W) LLS Inst GCV MS3 <br /> Isc : 1QMW-1B Multiplr 1 00 <br /> S Integration Params • lscint p <br /> 1 Quant Time May 17 07 28 . 58 2003 Quant Results File LLS0513 RES <br /> Quant Method C.\MSDCHEM\1\METHODS\LLS0513 .M (RTE Integrator) <br /> Title SW-846 Method 8260E WITH 5035 PURGE <br /> Last Update Wed May 14 09 . 58 : 12 2003 <br /> Response via Initial Calibration <br /> DataAcq Meth LLS0513 <br /> Internal Standards R T Qlon Response Conc Units Dev (Min) <br /> ----------- -- ---- --------------------------------- - -- --_--------- ---- ----- <br /> 1) Fluorobenzene 7 62 96 582159 10 00 ug/Kg 0 00 <br /> 43) Chlorobenzene-d5 12 . 17 117 370468 10 00 ug/Kg 0 . 00 <br /> 62) 1, 4-Dichlorobenzene-d4 15 85 152 181941 10 00 ug/Kg 0 00 <br /> System Monitoring Compounds <br /> 27) Dibromofluoromethane (SS) 6 61 113 69368 5 . 09 ug/Kg 0 . 00 <br /> 33) 1, 2-Dichloroethane-d4 (SS) 7 . 09 65 106485 5 . 60 ug/Kg 0 00 <br /> 36) 1, 4-Difluorobenzene (SS) 7 82 114 201831 4 . 31 ug/Kg 0 00 <br /> 44) Toluene-d8 (SS) 10 00 98 321626 5 22 ug/Kg 0 . 00 <br /> 61) 4-Bromofluorobenzene (SS) 14 . 02 95 116482 5 11 ug/Kg 0 . 00 <br /> 77) 1, 2-Dichlorobenzene-d4 (SS 16 .44 152 71213 4 05 ug/Kg 0 00 <br /> Target Compounds Qvalue <br /> 3) Chloromethane 1 77 50 1703 Below Cal # 69 <br /> 8) Ethanol 2 . 77 45 6662m Below Cal <br /> 10) Acetone 3 . 24 43 263542m 27 70 ug/Kg <br /> 12) Iodomethane 3 . 37 142 195 Below Cal # 41 <br /> 13) Methylene chloride 3 87 84 277 Below Cal # 1 <br /> 16) tert-Butyl Alcohol (TBA) 4 08 59 9020 Below Cal # 1 <br />' 19) Methyl-tert-Butyl Ether (M 4 . 34 73 60996m 1 . 00 ug/Kg <br /> 26) Chloroform 6 .46 83 29198 0 . 83 ug/Kg# 66 <br /> 31) Benzene 7 19 78 95083 1 10 ug/Kg 93 <br /> 34) 1, 2-Dichloroethane 7 21 62 156502 5 18 ug/Kg 94 <br /> 37) 1, 2-Dichloropropane 6 .48 63 861 0 04 ug/Kg# 62 <br /> 39) Bromodichloromethane 8 . 91 83 4117 0 . 17 ug/Kg 88 <br /> 40) 2--Chloroethyl vinyl ether 9 34 63 6761 15 . 69 ug/Kg# 1 <br /> 45) Toluene 10 10 92 16198 0 . 27 ug/Kg# 84 <br /> 48) 1, 1, 2-Trichloroethane 10 . 66 83 9709 0 . 66 ug/Kg# 1 <br /> 55) Ethylbenzene 12 .42 91 10795 0 11 ug/Kg 76 <br /> 56) m,p-Xylene 12 60 106 16781m 0 .44 ug/Kg <br /> 57) o-Xylene 13 .21 106 10147m 0 . 30 ug/Kg <br /> 60) Isopropylbenzene 13 . 81 105 68579 0 . 77 ug/Kg 96 <br /> 70) tert-Butylbenzene 15 . 25 119 100959 1 . 76 ug/Kg 99 <br /> 71) 1, 2, 4-Trimethylbenzene 15 34 105 7241m 0 11 ug/Kg <br /> 72) sec-Butylbenzene 15 . 62 105 72230 0 82 ug/Kg 93 <br /> 76) Benzyl Chloride 16 . 20 91 5572 0 . 12 ug/Kg# 70 <br /> ------------------------------------------- ------------------------------ <br /> (#) = qualifier out of range (m) = manual integration <br /> 05160347 D LLS0513 .M Thu May 22 15 11 . 16 2003 Page 1 <br />