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Wv4n. <br /> e 2852 Alton Ave Irvine CA 92606 (949)261 1022 FAX(949)261 1228 <br /> n� DSI Mar Analytical 1014E Cooley it 05 a Colton CA 92324 (909)370 4667 FAX(909)370 1048 <br /> 948a Chesapeake Or Suite 805 San[)sego CA 92123 (858)505 8596 FAX(858)505 9669 <br /> !4;es <br /> 9830 South 51st Si Suite 6 120 Phoenix AZ 85044 (480)785 0043 FAX(480)785 0851 <br /> 2520 E Sunset Atl #3 Las Vegas NV 89120 (702)796 3620 FAX(702)798 3621 <br /> Environmental Project ID 002-70950 Uhaul - Stockton <br /> 1433 North Third Avenue 2701 N Wilson Way Sampled 06/27/02 j <br /> Phoenix,AZ 85003 Report Number ILF141 1 Received 06/29/02 <br /> u Attention Brett McDaniel 1 <br /> METHOD BLANK/QC DATA <br /> BTEX/OXYGENATES by GC/MS (EPA 8260B) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Liuut Units Level Result %REC Linuts RPD Linut Qualifiers <br /> f1ch I2GO312 Extracted 07/03/02 <br /> atrix Spike Analyzed 07/03/02 (12G0302-MSI) Source ILGO080-01 <br /> Benzene 208 2 0 ug/l 25 0 ND 83 70-140 <br /> F <br /> thylbenzQne 220 2 0 ug/l 25 0 ND 88 75-135 <br /> oluene 21 2 2 0 ugll 25 0 ND 85 75-135 <br /> o-Xylene 21 0 2 0 ug/1 25 0 ND 84 75-150 <br /> m p-Xylenes 422 20 ug/l 500 ND 84 70-140 <br /> tylenes,Total 632 40 ug/l 75 0 ND 84 75-150 <br /> i-isopropyl Ether(DIPS) 239 5 0 ug/1 25 0 ND 96 65-135 <br /> Ethyl tent-Butyl Ether(ETBE) 226 5 0 ug/l 250 ND 90 65-135 <br /> e my[ Methyl Ether(TAME) 218 50 ug/1 25 0 ND 87 60-135 <br /> tert-butyl Ether(MTBE) 262 5 0 ug/l 250 5 9 81 65-150 <br /> to t- utanol(TBA) 118 50 ug/l 125 ND 94 55-160 <br /> arrogate Dibrorriofluoromethane 267 ugll 25 0 107 80-120 <br /> urrogate Toluene-d8 264 ugll 250 106 80 120 <br /> urrogate 4-Brotnofluorobenzene 262 ugll 250 105 80-120 <br /> ffdatrix Spike Dup Analyzed 07/03/02 (I2G0302-MSD1) Source ILGO080-01 <br /> enzene 230 20 ug/1 25 0 ND 92 70-140 10 20 <br /> thylbenzene 241 2 0 ug/1 25 0 ND 96 75-135 9 20 <br /> Toluene 23 3 2 0 ug/1 25 0 ND 93 75-135 9 20 <br /> t-Xylene 226 2 0 ug/l 25 0 ND 90 75-150 7 20 <br /> ,p-Xylenes 458 2 0 ug/1 500 ND 92 70-140 8 20 <br /> Xylenes,Total 684 40 ug/l 750 ND 91 75-150 8 20 <br /> '-isopropyl Ether(DIPE) 276 5 0 ug/1 25 0 ND 110 65-135 14 20 <br /> thyl tert-Butyl Ether(ETBE) 269 5 0 ugll 25 0 ND 108 65-135 17 20 <br /> tert-Amyl Methyl Ether(TAME) 264 5 0 ugll 25 0 ND 106 60-135 19 20 <br /> Ether(MTBE) 31 6 5 0 ug/l 25 0 5 9 103 65-150 19 20 <br /> rt-Butanol(TBA) 124 50 ug/l 125 ND 99 55-160 5 40 <br /> (elhy'-'ert-butyl <br /> rrogate Dibromofluoromethane 270 ugll 250 108 80-120 <br /> Surrogate Toluene-d8 263 ugll 250 105 80-120 <br /> urrogate 4-Bromofluorobenzene 264 ugll 25 0 106 80-120 <br /> 1 <br /> 0 <br /> L Mar Analytical, Irvine <br /> Y <br /> Jim Hatfield <br /> Iroject Manager <br /> The results pertain only to the samples tested in the laboratory This i eport shall not be reproduced <br /> except infull without written peninssion from Del MarAnalyucal ILF1411 .Page 39 of 46> <br />