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2852 Alton Ave Irvine CA 92606 (949)261 1022 FAX(949)261 1228 <br /> Del MarAnalytical 1014 E Cooley t 05 a C Diego CA 92324 (858)370 4667 FAX(909)370 1046 <br /> 9659 <br /> NY 9484 Chesapeake Or Suite 805 San Diego CA 92123 (658)505 6596 FAX(658)505 9669 <br /> -, 9830 South 5 t sl Sl Sune B 120 Phoenix AZ 85044 (480)785 0043 FAX(480)785 0851 <br /> 2520 E Sunset Rd 03 Las Vegas NV 69120 (702)796 3620 FAX(702)798 3621 <br /> es Em)ronniental Project ID 002-70950 Uhaui - Stockton _ <br /> 53 North Third Avenue 2701 N Wilson Way Sampled 03;06/02 <br /> Phoenix AZ 85003 Report Numbt-r ILCO402 Rcceived 03/04/02 <br /> Attention Brett McDaniel <br /> METHOD BLANK/QC DATA <br /> VOLATILE ORGANICS BY GC/MS (EPA 8260B) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch P20602 Extracted. 03/16/02 <br /> Matrix Spike Analyzed 03/16/02 (P2C1602-MSl) Source PLCO285-02 <br /> 1,2 4-Trimethylbenzene 263 20 ug/l 250 ND 105 75-120 <br /> 1,3,5-Trimethylbenzene 263 20 ug/l 250 ND 105 75-125 <br /> Vinyl chloride 264 50 ug/1 25 0 ND 106 70-150 <br /> o-Xylene 244 20 ug/1 250 ND 98 70-125 <br /> m p-Xylenes 51 7 20 ug/1 500 ND 103 70-125 <br /> Di-isopropyl Ether 248 50 ug/1 250 ND 99 65-135 <br /> Ethyl tertiary-Butyl Ether 255 50 ug/l 250 ND 102 65-135 <br /> Tert-Ainyl Methyl Ether 260 so ug/l 250 ND 104 60-135 <br /> Methyl-tert-butyl Ether(MTBE) 242 5 0 ug/1 25 0 ND 97 60-140 <br /> Thy-butanol 139 50 inti 125 ND 111 55-160 <br /> Sate DOIomofluoton)ethone 246 ttgll 250 98 80-735 <br /> Suttogate Toluene-d8 247 ugR 250 99 80-125 <br /> Stutogale 4-Hiotnoflunobcnzene 240 ttgll 250 96 75-125 <br /> Sut t ogate Dtbi oniollttot onlelhane 246 ug/l 2.) 0 93 80-115 <br /> Suttogate Toluene-d8 247 ug/1 250 99 80-125 <br /> Surrogate 4-Bromofluorobenzene 240 ttg/1 250 96 75-125 <br /> Matrix Spike Dup Analyzed 03/16/02 (P2C1602-MSDI) Source PLCO285-02 <br /> Benzene 25 l 2 0 ug/1 250 ND 100 70-125 4 20 <br /> Benzene 25 1 2 0 ug/l 250 ND 100 70-125 4 20 <br /> Ethylbenzene 255 2 0 ug/l 250 ND 102 75-135 4 20 <br /> Bromobenzene 254 5 0 ug/l 250 ND 102 75-125 3 20 <br /> Toluene 260 2 0 ug/l 250 ND 104 70-130 3 20 <br /> Bromochloromethane 268 5 0 ug/l 250 ND 107 70-130 1 20 <br /> m,p-Xylenes 495 2 0 ug/l 500 ND 99 70-125 4 20 <br /> Bromodlchloromethane 28 2 2 0 Ug/1 25 0 ND 113 70-130 2 20 <br /> o-Xylene 234 2 0 ug/l 25 0 ND 94 70-125 4 20 <br /> Bromoform 274 5 0 ug/1 25 0 ND 110 40-140 7 20 <br /> Total Xylenes 729 40 ug/l 75 0 ND 97 70-125 4 20 <br /> Bromomethane 256 5 0 ug/1 25 0 ND 102 65-150 3 20 <br /> Di-isopropyl Ether 245 5 0 ug/1 25 0 ND 98 65-135 1 20 <br /> Ethyl tertiary-Butyl Ether 260 5 0 ug/1 25 0 ND 104 65-135 7 20 <br /> n-Butylbenzene 240 5 0 ug/l 25 0 ND 96 80-125 5 20 <br /> Tert-Amyl Methyl Ether 268 5 0 ug/1 250 ND 107 60-135 3 20 <br /> Methyl-tert-butyl Ether(MTBE) 26 7 5 0 ug/l 250 ND 107 60-140 10 20 <br /> lbenzene 24 4 5 0 ug/l l 25 0 ND 98 75-130 4 20 <br /> to rylbenzene 246 5 0 ug/1 25 0 ND 98 75-130 4 20 <br /> Del Mar Analytical,Irvine <br /> Jim Hatfield <br /> Protect Manager <br /> The results pet taut only to the samples tested rtr the labor atop-i, This report shall not be rep oduced <br /> except ut/till it lthout 1t;then pet mission T ont Del Itat Analvucal ILCO402 <Page 45 of 49> <br />