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2852 Allon Ave Irvine CA 92606 (949)261 1022 FAX(949)261 1228 <br /> Del MarAnalytical 7014E Crst S1 Suite A Colton CA 92324 (909)370 4867 FAX(909)370 1048 <br /> 7277 Hayvenhurs[ Suite B 12 Van Nuys CA 91406 (618)779 1844 FAX(818}779 1843 <br /> 9484 Chesapeake Or Suite 805 San Diego CA 92123 (858)505 9596 FAX(858)505 9589 <br /> 9830 South 51 st SI Suite 6 120 Phoerox AZ 85044 (480)785 0043 FAX(480)785 0851 <br /> -� �_,. 1.,1r�.�v�a.�ssa:n:rr�.-.x:�rR�.,,+ax.xv^errr�.+m�:�-we�+•�auc,., -.�.,.�..-�� <br /> laes Environmental Project ID 002-70950 Uhaul - Stockton <br /> 433 North Third Avenue 2701 N Wilson Way Sampled 09/25/01-09/26/01 <br /> Phoenix, AZ 85003 Report Number IKI1072 Received 09/29/01 <br /> Attention Brett McDaniel <br /> METHOD BLANK/QC DATA <br /> BTEX/OXYGENATES by GOMS (EPA 8260B) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch, 1113004 Extracted, 09/30/01 <br /> Matrix Spike Analyzed 09/30/01 (1113004-MSI) Source IK11072-05 <br /> Benzene 248 20 ug/l 250 ND 986 70-140 <br /> Ethylbenzene 246 20 ug/1 250 ND 972 80-135 <br /> Toluene 248 20 ug/I 250 ND 978 75-135 <br /> o-Xylene 259 20 ug/l 250 ND 104 75-150 <br /> m,p-Xylenes 525 20 ug/l 500 ND 103 70-140 <br /> Xylenes,Total 784 40 ug/1 750 ND 103 75-150 <br /> Di-isopropyl Ether(DIPS) 215 50 ug/I 250 ND 860 65-135 <br /> Ethyl tert-Butyl Ether(ETBE) 22 7 50 ugrt 250 ND 908 65-135 <br /> tert-Amyl Methyl Ether(TAME) 242 so ug/I 250 ND 968 60-135 <br /> allyl-tert-butyl Ether(MTBE) 252 50 ug/l 250 ND 101 65-150 <br /> utanol(TBA) 130 50 ug/I 125 ND 104 55-160 <br /> Surrogate Dtbromofluoromethane 231 ugll 250 924 80-120 <br /> Surrogate Toluene-d8 230 ttgll 250 920 80-120 <br /> Surrogate 4-Bromofluorobenzene 236 ugll 250 944 80-120 <br /> Matrix Spike Dup Analyzed 09/30/01 (I1I3004-MSDI) Source IKI1072-05 <br /> Benzene 27 8 20 ug/I 250 ND 111 70-140 11 4 20 <br /> Ethylbenzene 276 20 ug/l 250 ND 109 80-135 11 5 20 <br /> Toluene 27 8 20 ug/l 250 ND 110 75-135 11 4 20 <br /> o-Xylene 290 20 ug/l 250 ND 116 75-150 11 3 20 <br /> m,p-Xylenes 592 20 ug/l 500 ND 117 70-140 120 20 <br /> Xylenes,Total 882 40 ug/I 750 ND 116 75-150 11 8 20 <br /> Di-isopropyl Ether(D1PE) 245 50 ug/l 250 ND 980 65-135 13 0 20 <br /> Ethyl tert-Butyl Ether(ETBE) 25 6 50 ug/I 250 ND 102 65-135 120 20 <br /> tent-Amyl Methyl Ether(TAME) 264 50 ug/l 250 ND 106 60-135 870 20 <br /> Methyl-tent-butyl Ether(MTBE) 27 3 50 ug/l 250 ND 109 65-150 800 20 <br /> tert-Butanol(TBA) 149 50 ua/I 125 ND 119 55-160 13 6 40 <br /> Stu rugate Dtbromofluoromethane 236 ttgll 250 944 80-120 <br /> Surrogate Toluene-d8 230 ttgll 250 920 80-120 <br /> Surrogate 4-Brornoflitwobenzene 235 ugll 250 940 80-120 <br /> 0 <br /> Del Mar Analytical, Irvine <br /> Jim Hatfield <br /> Project Manager <br /> The t esults pertain onlv to the samples tested in the labor atony This i epos t shall nor be t eproduced <br /> elcepr rnfull without ut itten pemussion from Del Afar Analytical IKII072 <Page 24 of 33> <br />