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2852 Alton Ave Irvine CA 92606 (949)261 1022 FAX{949}261 1228 <br /> 1014 S Coldby or Suite A Colton CA 92324 (909)370 4667 PAX{909{370 1046 <br /> Del Mar Analytical 7277 ar Suite B 12 Van Nuys CA 91406 (818)779 1844 FAX(818)779 1843 <br /> 9464 Chessapeakepeake Drr Suite 805 San Diego CA 92423 (858)505 8596 FAX(856)505 9569 <br /> 9830 South 51 st St Suite B 120 Phoenix AZ 85044 (480)785 0043 FAX(460)785 0851 <br /> tAttention <br /> aes Environmental Project ID 002-70950 Uhaul - Stockton <br /> 33 North Third Avenue 2701 N Wilson Way Sampled 09125101-09126101 <br /> oenix, AZ 85003 Report Number 1KI1072 Received 09/29/01 <br /> Brett McDaniel <br /> METHOD BLANK/QC DATA <br /> BTEX/OXYGENATES by GC/MS (EPA 8260B) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch. 11 J031.0Ertracted. 10/03/01 <br /> Matrix Spike Analyzed 10/03/01 (I1J0310-MSI) Source IKI1017-05 <br /> Benzene 276 2 0 ug/I 250 ND 109 70-140 <br /> Ethylbenzene 276 2 0 ug/I 250 ND 109 80-135 <br /> Toluene 121 2 0 ug/I 250 99 880 75-135 <br /> o-Xylene 28 4 2 0 ug/I 25 0 ND 111 75-150 <br /> rn,p-Xylenes 583 2 0 ug/l 500 ND 114 70-140 <br /> Xylenes,Total 866 4 0 ug/1 750 ND 113 75-150 <br /> Dt-isopropyl Ether(RIPE) 275 5 0 ug/1 250 ND 110 65-135 <br /> Ethyl tert-Butyl Ether(ETBE) 277 5 0 ug/I 250 t,D 111 65-135 <br /> tert-Amyl Methyl Ether(TAME) 27 l 5 0 ug/I 250 ND 108 60-135 <br /> V1-tert-butyl Ether(MTBE) 276 5 0 ug/1 250 ND 107 65-150 <br /> utanol(TBA) 129 50 ug/I t25 ND 103 55-160 <br /> Surrogate Dibrontofluoromethane 268 11gll 250 107 80-120 <br /> Surrogate Toluene-d8 267 ugll 250 107 80-120 <br /> Surrogate 4-Bromofluorobenzene 258 ugll 250 103 80-120 <br /> Matrix Spike Dup Analyzed 10/03/01 (I1J0310-MSD1) Source IKI1017-05 <br /> Benzene 290 2 0 ug/I 250 ND 115 70-140 495 20 <br /> Ethylbenzene 295 2 0 ug/I 250 ND 117 80-135 665 20 <br /> Toluene 124 2 0 ug/I 25 0 99 100 75-135 245 20 <br /> o-Xylene 29 8 2 0 ugll 25 0 ND 117 75-150 4 81 20 <br /> m,p-Xylenes 61 8 2 0 ug/I 500 ND 121 70-140 5 83 20 <br /> Xylenes,Total 91 6 4 0 ug/I 750 ND 120 75-150 5 61 20 <br /> D1-isopropyl Ether(DIPE) 29 1 5 0 ug/i 25 0 ND 116 65-135 5 65 20 <br /> Ethyl tert-Butyl Ether(ETBE) 29 9 5 0 ug/I 250 ND 120 65-135 764 20 <br /> tert-Amyl Methyl Ether(TAME) 287 5 0 ug/I 250 ND 115 60-135 5 73 20 <br /> Methyl-tert-butyl Ether(MTBE) 29 9 5 0 ug/l 250 ND 116 65-150 800 20 <br /> tert-Butanol(TBA) 137 50 ug/I 125 ND 110 55-160 602 40 <br /> 51a rogate Dtbi otnofluoroniethane 264 ugll 250 106 80-120 <br /> Surrogate Toluene-d8 268 ugll 25 0 107 80-120 <br /> Surrogate 4-81 oinofluorobenzene 258 iigll 250 103 80-120 <br /> 0 <br /> )eI Mar Analytical, Irvine <br /> im Hatfield <br /> 'rod ect Manager ► <br /> The tesnits pet tarn only to the samples tested ur the laboratory This t epos t shall not be rept oduced <br /> except ur fidt it uhout it r ttten per nusston fr ont De1,Ylai Analytical IKI1072 <Paee 32 of 33> <br />