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I 10 Second Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampE gll coin E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Protect ID Top Filling Date Sampled 06/12/98 <br /> 4005 North Wilson Way Date Received 06/17/98 <br /> Stockton,CA 95205 Client Contact Tim Cuellar Date Extracted 06119-06/20/98 <br /> IClient P O Date Analyzed 06/19-06/20/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab M 90574 <br /> Client ID M W 116-12-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND4 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl 1,etone' ' ND <br /> Bromomethane ND Methylene Chloride"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone'' ND <br /> sec-Butyl benzene ND Methyl isobut)I ketone's ND <br /> tent-Butyl benzene ND Methyl tert-Butt'I Ether(MTBE) --- <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene` ND <br /> Chloroethane ND 1,1,12-Tetrachloroethane ND <br />' 2-Chloroethyl Vinyl Ether` ND 1,1 2 2-Teir2clitoroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 1 2 3-Trichiorobenzene ND <br /> 4-Chlorotoluene ND 1 2 4-Trichlorobenzene ND <br /> Dibromochloromethane ND 1,1 I-Tiichloroethane ND <br /> l2-Dibromo-3-chloropropane ND 112-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br />' 12-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 12,3-Tiichlompropane ND <br /> 1,4-Dichlorobenzene ND 1,2 4-Trimcthylbenzene ND <br /> Dichlorodifluoromethane ND 1 3 5-Tnmethvlbenzene ND <br />' 1,1-Dichloroethane ND Vinyl Acetate""' ND <br /> 1,2-Dichloroethane ND Vinyl Chloride"' NO <br /> 1,1-Dichloroethene ND Xylenes total '°' ND <br />' cis-1,2-Dichloroethene ND <br /> trans-l,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1 3-Dichloropropane ND <br />' 2,2-Dichloropropane ND Comments <br /> IJ-Dichloropropene ND Surrogate RecoN cries(%) <br /> cis-13-Dichloropropene ND Dibromotluoromethane 106 <br /> trans-l,3-DichIoropropene ND Toluene-d8 101 <br />' Ethylene dibromide ND 4-Bromofluorobenzene 91 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in uglwtpe and all TCLP!SPLP extracts to ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ugiL .apor samples 05 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 2uglwipe ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (t) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (t) liquid sample that contains greater than—5 voi % <br /> sediment 0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester (n)chloroe.thene (o)dimethylbenzenes <br />' DHS Certification No 1644 Edward Hamilton,Lab Director <br />