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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 17605 242 5•717-656-2300 Fax 717-656-2661 wWW IariCaSterlab5 GOrrk 0 <br /> Page 3 of 3 <br /> Quality Control Summary <br /> Client Name ChevronTexacc c/o SECOR Group Number 904094 <br /> Reported 07/27/04 at 12 57 PM <br /> Surrogate Quality Control <br /> Dibromoflucromethane 1 2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4312580 109 104 107 103 <br /> Blank 110 107 106 104 <br /> LCS 107 102 107 105 <br /> NES 107 102 99 99 <br /> MSD 107 103 101 99 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX+5 Oxygenates+EDC+EDS+ETOH <br /> Batch number Z042041AA <br /> Dibromoflucromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4312581 99 101 97 89 <br /> 4312582 98 100 97 88 <br /> 4312583 98 100 97 88 <br /> 4312584 99 100 98 88 <br /> Blank 101 107 99 89 <br /> LCS 99 104 98 95 <br /> MS 98 103 98 93 <br /> MSD 98 102 97 93 <br /> Limits 81-120 82-112 85-112 83-113 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the splice added <br />