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oilLancaster <br /> . . LAba�aboratories Analysis Report <br /> 5 New Holland Pike,PO Boot 12425 Lancasler,PA 17605-2425.717 6562300 Fax 717-656-2681•www laneasterlabs com <br /> Page l of 4 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 869558 <br /> Reported 10/16/03 at 01 17 PM <br /> Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Resul MDL Units %REC Limits RPD RPD Max <br /> Batch number 03279A56A Sample number(s) 4136922-4136927 <br /> TPH-GRO - Waters N D 50 ug/1 96 98 70-130 2 30 <br /> Batch number 032SIA07B Sample number(s) 4136920 <br /> TPH-GRO - Waters N D 50 ug/1 104 70-130 <br /> Batch number 032820024A Sample number(s) 4136921-4136923 <br /> Methanol (by Direct Injection) N D 1000 ug/1 92 78-114 <br /> Batch number 032820025A Sample number(B) 4136924-4136927 <br /> Methanol (by Direct Injection) N D 1000 ug/1 92 78-114 <br /> Batch number 03262A07A Sample number s) 4136921 <br /> TPH-GRO - Waters N D 5o ug/1 97 114 70-130 16 30 <br /> Batch number P032811AA Sample number($) 4136921-4136927 <br /> Ethanol N D 500 ug/l 74 46-145 <br /> Methyl Tertiary Butyl Ether N D 2 ug/1 99 77-127 <br /> di-Isopropyl ether N D 2 1,19/1 99 74-125 <br /> Ethyl t-butyl ether N D 2 ug/l 100 74-120 <br /> Amyl methyl ether N D 2 ug/l 98 79-113 <br /> utyl alcohol N D 100 ug/l 89 53-147 <br /> nzene N D 5 ug/l 103 85-117 <br /> ,2-Dichloroethane N D 2 ug/l 99 77-132 <br /> Toluene N D 5 ug/l 97 85-115 <br /> 1,2-Dibromoethane N D 2 ug/l 92 81-114 <br /> Ethylbenzene N D 5 ug/l 97 82-119 <br /> Xylene (Total) N D 5 ug/l 98 84-120 <br /> Batch number P032822AA Sample number(s) 4136920 <br /> Methyl Tertiary Butyl Ether N D 2 ug/1 107 77-127 <br /> Benzene N D 5 ug/1 113 85-117 <br /> Toluene N D 5 ug/1 110 85-115 <br /> Ethylbenzene N D 5 ug/1 109 82-119 <br /> Xylene (Total) N D 5 ug/1 109 84-120 <br /> Sample Matrix Quality Control <br /> MS MSA M&/MSD RPD BRG DUP Dire Dup <br /> RPD <br /> Analysis Name %R6C %RSC Limits RPD MAX Cona Cone RPD Max <br /> Batch number 03279A56A Sample number(s) 4136922-4136927 <br /> TPH-GRO - Waters 116 63-154 <br /> Batch number 03281A07B Sample number(s) 4136920 <br /> TPH-GRO - Waters 117 119 63-154 2 30 <br /> Batch number 032820024A Sample numbers) 4136921-4136923 <br /> Methanol (by Direct Injection) 92 88 73-117 4 20 <br /> Batch number 032820025A Sample numbers) 4136924-4136927 <br /> Methanol (by Direct Injection) 92 92 73-117 0 20 <br /> *-Outside of specification <br /> The result for one or both determinations was less than five times the LOQ <br /> , ) <br /> The background result was more than four times the spike added <br />