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Analysis Report <br /> lipLancaster Laporaiones Pagel oft <br /> Where quality�s a s len e <br /> Qua ity EonVrol Summary <br /> Client Name Chevron Products Company Group Number 792545 <br /> Reported: 01/21/02 at 09 02 PM <br /> Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LC$/LCSD <br /> Analysis Name _ _ Result _ MDL__Unsts__- %REC _%REC Limits _ RPD_ RPD Max <br /> Batch number 02009A55 Sample number(s) 3754674--3754677 <br /> Benzene N D 0 5 ug/1 107 102 80-118 4 30 <br /> Toluene N D 0 5 ug/l 111 108 82-119 _ 3 30 <br /> Ethylbenzene N D 0 5 ug/1 114 111 81-119 2 30 <br /> Total Xylenes N D 1 5 ug/1 113 110 82-120 2 30 <br /> Methyl tert-Butyl Ether N D 2 5 ug/l 104 103 79-127 0 30 <br /> TPH-GRO - Waters N D 50 ug/l 90 86 76-119 5 20 <br /> Batch number 020110001A Sample number(s) 3754 67 5-3754 677 <br /> Methanol (by Direct Injection) N D 1000 ug/l 96 80-113 <br /> Batch number V020091AB Sample number(s) 3754675-3754677 <br /> Ethanol N D 500 ug/l 99 44-139 <br /> Methyl t-butyl ether N D 2 ug/1 106 77-127 <br /> di-Isopropyl ether N D 2 ug/l 108 74-125 <br /> Ethyl t-butyl ether N D 2 ug/l 107 74-120 <br /> t-Amyl methyl ether N D 2 ug/l 107 71-119 <br /> t-Butyl alcohol N D 100 ug/l 116 59.139 <br /> Sample Matrix Qualxty Control • <br /> MS MSD M3/MSD RPD BICC DUP - DUP Dup <br /> RPD <br /> Analysis Name %REG $REC Limits RPD MAX Cone Cone RPD Max <br /> Batch number 02009A55 Sample number(s) 3754674-3754677 <br /> Benzene 109 110 66=190 1 30 <br /> Toluene 115 115 72-138 0 30 <br /> _ Ethylbenzene - -- 118 11B-71-138-0 71-138 0 30�� <br /> Total Xylenes 117 117 69-140 0 30 <br /> Methyl tert-Butyl Ether 95 105 60-145 6 30 <br /> - ---TPH-GRO—Waters _T- --- -- 108 -=109 -T74-132 -- - - 20 <br /> Batch number 020110001A Sample numbers) 3754675-3754677 <br /> Methanol (by Direct Injection) 96 96 76-114 0 20 <br /> Batch number V020091AB Sample numberts) 3754675-3754677 <br /> Ethanol 96 92 70-130 4 30 <br /> Methyl t-butyl ether 98 96 69-134 2 30 <br /> di-Isopropyl ether 102 97 68-133 5 30 <br /> Ethyl -t-butyl ether 101 97 73-123 4 30 <br /> t-Amyl methyl ether 100 97 69-118 3 30 <br /> t-Butyl alcohol 100 96 51-148 4 30 <br /> Surrogate Quality Control <br /> *- Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br /> Lancaster Laboratories Inc <br /> M E M B E R 2425 New Holland Pike <br /> PO Box 12425 <br /> Lancaster PA 17605-2425 <br /> 717-656 2300 Fax 717-656 2681 2216 Rev 9/11/00 <br />