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GeoAnalytical Laboratories, Inc. <br />' 1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> port# N323-12 <br /> CERTIFICATE OF ANALYSIS Date 11/25/02 <br /> J Kloberdanz & Associates Date Recd 11/19/02 <br /> Date Started 11/22/02 <br /> P O Box 576981 Project Ripona Market Date Completed 11/22/02 <br /> Modesto CA 95357 <br /> Date Sampled 11/19/02 <br /> PO# Time 1120 am <br /> Sample 1Sampler M J Kloberdanz <br /> Lab ID q;;Z;EE:) <br />' Method RL Analyte Results Units _ <br /> 82605 03 Benzene ND pg/L <br /> 0 3 Toluene 1 1 <br /> 0 3 Ethyl Benzene ND <br /> 0 6 Total Xylenes ND <br /> 1 0 Methyl tert-butyl ether(MTBE) ND <br /> 40 Ethanol ND <br /> 20 tert-Butanol ND <br /> 1 0 di-Isopropyl ether(RIPE) ND <br /> 1 0 Ethyl tert-butyl ether (ETBE) ND <br /> 1 0 tert-Amyl methyl ether(TAME) ND <br /> 1 0 Ethylene dibromide(EDB) ND <br /> 0 5 1,2-Dichloroethane (1,2-DCA) ND <br /> I Surrogate Arrint Spiked Amnt Rec %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 5 00 4 61 922 72-132 <br /> 2-Bromo 1-chloropropane 5 00 4 75 95 0 71-134 <br /> 4-Bromofluorobenzene 5 00 4 86 972 74-132 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />